Development and applications of a sample controlled DSC system

The development of a new sample controlled thermal analysis technique based on a heat flux DSC is described. The performance of the system is demonstrated by studies on the decomposition of sodium bicarbonate and the oxidation of a copper impregnated carbon. The ability of the technique to study rea...

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Bibliographic Details
Published in:Journal of thermal analysis and calorimetry 2011-08, Vol.105 (2), p.699-703
Main Authors: Charsley, E. L., Laye, P. G., Parkes, G. M. B., Rooney, J. J.
Format: Article
Language:English
Subjects:
Analytical Chemistry
Applied sciences
Calorimetry
Carbon
Carbonates
Chemical properties
Chemistry
Chemistry and Materials Science
Curing
Differential scanning calorimetry
Epoxy resins
Exact sciences and technology
Heat flux
Inorganic Chemistry
Measurement Science and Instrumentation
Physical Chemistry
Polymer industry, paints, wood
Polymer Sciences
Properties and testing
Sodium bicarbonate
Technology of polymers
Thermal analysis
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Description
Summary:The development of a new sample controlled thermal analysis technique based on a heat flux DSC is described. The performance of the system is demonstrated by studies on the decomposition of sodium bicarbonate and the oxidation of a copper impregnated carbon. The ability of the technique to study reactions which take place without a change in mass is illustrated by the curing of an epoxy resin with a polyaminoamide hardener.
ISSN:1388-6150
1588-2926
1572-8943
DOI:10.1007/s10973-010-1196-8