Mechanical properties and multiscale characterization of nanofiber-alumina/epoxy nanocomposites

In contrast to the bulk of published nanocomposite studies, in this study we investigated the mechanical properties of alumina/epoxy nanocomposites manufactured with nanofillers having a fiber or whisker morphology. The article describes how ultrasonic dispersion and in situ polymerization were used...

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Bibliographic Details
Published in:Journal of applied polymer science 2011-02, Vol.119 (3), p.1459-1468
Main Authors: Brown, G. M., Ellyin, F.
Format: Article
Language:English
Subjects:
Aluminum oxide
Applied sciences
Composites
Exact sciences and technology
Fibers
Forms of application and semi-finished materials
Materials science
Mechanical properties
microstructure
Nanocomposites
Nanomaterials
Nanoparticles
Nanostructure
particle size distribution
Polymer industry, paints, wood
Polymerization
Polymers
structure-property relations
Technology of polymers
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Summary:In contrast to the bulk of published nanocomposite studies, in this study we investigated the mechanical properties of alumina/epoxy nanocomposites manufactured with nanofillers having a fiber or whisker morphology. The article describes how ultrasonic dispersion and in situ polymerization were used to incorporate these 2–4 nm diameter fibers (with aspect ratios of 25–50) into a two‐part epoxy resin (Epon 826/Epicure 9551). The use of untreated and surface‐modified nanoparticles is contrasted, and improvements in both the tensile strength and modulus were observed at low filler loadings. Microstructural characterization of the nanocomposites via multiscale digital image analysis was used to interpret the mechanical properties and was found to be useful for direct comparison with other nanocomposites. In addition, superior performance was demonstrated through comparisons with numerous nanocomposites with nanoparticle reinforcements ranging from carbon nanofibers to spherical alumina particles. © 2010 Wiley Periodicals, Inc. J Appl Polym Sci, 2011
ISSN:0021-8995
1097-4628
1097-4628
DOI:10.1002/app.32662