Synthesis and study of sodium vanadomanganate

Sodium 13-vanadomanganate Na7[MnV13O38]DT5H2O (I) has been synthesized and studied by mass spectrometry, thermogravimetry, IR spectroscopy, and X-ray powder diffraction analysis. The crystals of compound I are monoclinic: a = 11.487 A, b = 7.613 A, c = 11.359 A, b = 114.15DG, V = 906.52 A, rcalcd =...

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Bibliographic Details
Published in:Russian journal of inorganic chemistry 2007-12, Vol.52 (12), p.1864-1867
Main Authors: Kaziev, G. Z., Oreshkina, A. V., Holguin Quinones, S., Glazunova, T. Yu, Alekseev, D. A., Cruz Fernandez, E. G.
Format: Article
Language:English
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Summary:Sodium 13-vanadomanganate Na7[MnV13O38]DT5H2O (I) has been synthesized and studied by mass spectrometry, thermogravimetry, IR spectroscopy, and X-ray powder diffraction analysis. The crystals of compound I are monoclinic: a = 11.487 A, b = 7.613 A, c = 11.359 A, b = 114.15DG, V = 906.52 A, rcalcd = 2.73 g/cm, Z = 1.
ISSN:0036-0236
1531-8613
DOI:10.1134/S0036023607120108