Atom-economical synthesis of 3,3,3-trifluoropropanal dialkyl acetals through Pd/C catalyzed acetalization of 3,3,3-trifluoropropene

A facile and efficient procedure for one-step synthesis of 3,3,3-trifluoropropanal dialkyl acetals from readily available 3,3,3-trifluoropropene (TFP) has been developed. The catalyst can be recycled for 4 times without obvious deactivation. This process provides a novel and atom-economical syntheti...

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Bibliographic Details
Published in:RSC advances 2016-01, Vol.6 (45), p.39387-39391
Main Authors: Kang, Jian-Ping, Lu, Ju-You, Li, Yang, Wang, Zhi-Xuan, Mao, Wei, Lu, Jian
Format: Article
Language:English
Subjects:
Acetals
Catalysts
Deactivation
Palladium
Recycled
Strategy
Synthesis
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Summary:A facile and efficient procedure for one-step synthesis of 3,3,3-trifluoropropanal dialkyl acetals from readily available 3,3,3-trifluoropropene (TFP) has been developed. The catalyst can be recycled for 4 times without obvious deactivation. This process provides a novel and atom-economical synthetic strategy for the preparation of functional CF 3 -containing compounds.
ISSN:2046-2069
2046-2069
DOI:10.1039/C6RA03208G