Synthesis, Molecular, and Crystal Structure of 4,6-Dinitro-5,7-dichloro-2,1,3-oxadiazole-1-oxide

A new convenient method for the preparation of dichlorodinitro-2,1,3-oxadiazole-1-oxide (dichlorodinitrobenzofuroxan) has been developed. Composition and structure of the prepared dichlorodinitrobenzofuroxan have been elucidated by a set of chemical, physical, and physico-chemical methods and also c...

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Bibliographic Details
Published in:Russian journal of general chemistry 2022-12, Vol.92 (12), p.2555-2560
Main Authors: Galkina, I. V., Yusupova, L. M., Bakhtiyarov, D. I., Gerasimov, A. V., Islamov, D. R., Litvinov, I. A., Bakhtiyarova, Yu. V.
Format: Article
Language:English
Subjects:
Chemical synthesis
Chemistry
Chemistry and Materials Science
Chemistry/Food Science
Crystal structure
Crystals
Diffraction
Molecular structure
Oxadiazoles
Single crystals
Stability analysis
Structure
Thermal stability
Thermogravimetry
X-rays
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Summary:A new convenient method for the preparation of dichlorodinitro-2,1,3-oxadiazole-1-oxide (dichlorodinitrobenzofuroxan) has been developed. Composition and structure of the prepared dichlorodinitrobenzofuroxan have been elucidated by a set of chemical, physical, and physico-chemical methods and also confirmed for the first time via single crystal X-ray diffraction analysis. Thermal stability of the compound has been investigated using a method of combined thermogravimetry and differential scanning calorimetry.
ISSN:1070-3632
1608-3350
DOI:10.1134/S1070363222120015