Synthesis and structure of 3-substituted 1,5-dinitro-1,3,5-triazepanes

A method has been optimized for the condensation of ethylenedinitroamine with aliphatic amines and formalaldehyde, leading to the formation of 3-alkyl-1,5-dinitro-1,3,5-triazepanes. The structure of the obtained 1,3,5-triazepanes was studied by multinuclear NMR and X-ray structural analysis.

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Bibliographic Details
Published in:Chemistry of heterocyclic compounds (New York, N.Y. 1965) N.Y. 1965), 2022-09, Vol.58 (10), p.500-505
Main Authors: Gribov, Pavel S., Frank, Dmitry F., Getmanova, Anfisa D., Suponitsky, Kyrill Yu, Sheremetev, Aleksei B.
Format: Article
Language:English
Subjects:
Aliphatic amines
Amines
Chemistry
Chemistry and Materials Science
NMR
Nuclear magnetic resonance
Organic Chemistry
Pharmacy
Structural analysis
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Summary:A method has been optimized for the condensation of ethylenedinitroamine with aliphatic amines and formalaldehyde, leading to the formation of 3-alkyl-1,5-dinitro-1,3,5-triazepanes. The structure of the obtained 1,3,5-triazepanes was studied by multinuclear NMR and X-ray structural analysis.
ISSN:0009-3122
1573-8353
DOI:10.1007/s10593-022-03119-1