Micro-scale Synthesis and In-Situ Spectroscopic Characterization of Some Chemical Weapons Related Organophosphonate Compounds

Inspection protocols for the Chemical Weapons Treaty, which went into effect on April 29, 1997 require on-site analytical procedures which include a comprehensive mass spectral database of hundreds of scheduled compounds. A number of these compounds were prepared on a nanogram scale via a micro-scal...

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Bibliographic Details
Published in:Analytical letters 1998-06, Vol.31 (8), p.1429-1444
Main Authors: Durst, H. Dupont, Mays, Jeffrey R., Ruth, Jill L., Williams, Barry R., Duevel, Robert V.
Format: Article
Language:English
Subjects:
Analytical chemistry
Chemical Weapons
Chemistry
Chromatographic methods and physical methods associated with chromatography
Exact sciences and technology
Gas chromatographic methods
Infrared Spectroscopy
Mass Spectrometry
Methylphosphonofluoridates
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Summary:Inspection protocols for the Chemical Weapons Treaty, which went into effect on April 29, 1997 require on-site analytical procedures which include a comprehensive mass spectral database of hundreds of scheduled compounds. A number of these compounds were prepared on a nanogram scale via a micro-scale synthetic approach using GC-IRD/MSD analytical instrumentation to purify and identify the resulting products. The collected electron impact mass spectra will be made available for use in relevant databases.
ISSN:0003-2719
1532-236X
DOI:10.1080/00032719808002877