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Construction of Sensor for Submicromolar Detection of Riboflavin by Surface Modification of SPCE with Thermal Degradation Products of Nickel Acetate Tetrahydrate
Nickel acetate tetrahydrate (NAT) sample series were used to modify screen‐printed carbon electrodes (SPCE). The samples were hybrid Ni/NiO nanocomposites, where the NiO phase increased with an applied treatment temperature. Results of electrochemical measurements pointed that the Ni/NiO550/SPCE‐mod...
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Published in: | Electroanalysis (New York, N.Y.) N.Y.), 2022-09, Vol.34 (9), p.1431-1440 |
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Main Authors: | , , , , , , , |
Format: | Article |
Language: | English |
Subjects: | |
Citations: | Items that this one cites Items that cite this one |
Online Access: | Get full text |
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Summary: | Nickel acetate tetrahydrate (NAT) sample series were used to modify screen‐printed carbon electrodes (SPCE). The samples were hybrid Ni/NiO nanocomposites, where the NiO phase increased with an applied treatment temperature. Results of electrochemical measurements pointed that the Ni/NiO550/SPCE‐modified electrode had the best analytical performance toward the detection of riboflavin (RF). The Ni/NiO550/SPCE‐based sensor showed linear response with RF in the concentration range of 0.5–75 μM and 0.15 μM LOD in BRBS. Sensor offered fast response time, good repeatability, and selectivity with an RSD of 1.4 %. Our results show that the Ni:NiO nanocomposite ratio strongly influenced the electroanalytical performance of SPCE. |
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ISSN: | 1040-0397 1521-4109 |
DOI: | 10.1002/elan.202100602 |