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Nucleation and crystallization of tailing-based glass-ceramics by microwave heating

The effect of microwave radiation on the nucleation and crystallization of tailing-based glass-ceramics was investigated using a 2.45 GHz multimode microwave cavity. Tailing-based glass samples were prepared fi'om Shandong gold tailings and Guyang iron tailings utilizing a conventional glass melting...

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Published in:International journal of minerals, metallurgy and materials metallurgy and materials, 2015-12, Vol.22 (12), p.1342-1349
Main Authors: Li, Bao-wei, Li, Hong-xia, Zhang, Xue-feng, Jia, Xiao-lin, Sun, Zhi-chao
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Language:English
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description The effect of microwave radiation on the nucleation and crystallization of tailing-based glass-ceramics was investigated using a 2.45 GHz multimode microwave cavity. Tailing-based glass samples were prepared fi'om Shandong gold tailings and Guyang iron tailings utilizing a conventional glass melting technique. For comparison, the tailing-based glass samples were crystallized using two different heat-treatment methods: conventional heating and hybrid microwave heating. The nucleation and crystallization temperatures were determined by performing a differential thermal analysis of the quenched tailing-based glass. The prepared glass-ceramic samples were further characterized by Fourier transform infrared spectroscopy, X-ray diffraction, Raman spectroscopy, thermal expansion coefficient measurements, and scanning electron microscopy. The results demonstrated that hybrid microwave heating could be successfully used to crystallize the tailing-based glass, reduce the processing time, and decrease the crystallization temperature. Furthermore, the results indicated that the nucleation and crystallization mechanism of the hybrid microwave heating process slightly differs fi'om that of the conventional heating process.
doi_str_mv 10.1007/s12613-015-1203-y
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Tailing-based glass samples were prepared fi'om Shandong gold tailings and Guyang iron tailings utilizing a conventional glass melting technique. For comparison, the tailing-based glass samples were crystallized using two different heat-treatment methods: conventional heating and hybrid microwave heating. The nucleation and crystallization temperatures were determined by performing a differential thermal analysis of the quenched tailing-based glass. The prepared glass-ceramic samples were further characterized by Fourier transform infrared spectroscopy, X-ray diffraction, Raman spectroscopy, thermal expansion coefficient measurements, and scanning electron microscopy. The results demonstrated that hybrid microwave heating could be successfully used to crystallize the tailing-based glass, reduce the processing time, and decrease the crystallization temperature. Furthermore, the results indicated that the nucleation and crystallization mechanism of the hybrid microwave heating process slightly differs fi'om that of the conventional heating process.</description><identifier>ISSN: 1674-4799</identifier><identifier>EISSN: 1869-103X</identifier><identifier>DOI: 10.1007/s12613-015-1203-y</identifier><language>eng</language><publisher>Beijing: University of Science and Technology Beijing</publisher><subject>Ceramics ; Characterization and Evaluation of Materials ; Chemistry and Materials Science ; Composites ; Corrosion and Coatings ; Crystallization ; Differential thermal analysis ; Fourier transforms ; Glass ; Glass ceramics ; Heat treatment ; Heating ; Infrared spectroscopy ; Materials Science ; Metallic Materials ; Microwave heating ; Microwave radiation ; Microwaves ; Mine tailings ; Natural Materials ; Nucleation ; Raman spectroscopy ; Spectrum analysis ; Surfaces and Interfaces ; Tailings ; Thermal analysis ; Thermal expansion ; Thin Films ; Tribology ; X-ray diffraction ; X射线衍射仪 ; 傅里叶变换红外光谱 ; 尾矿微晶玻璃 ; 微波加热 ; 扫描电子显微镜 ; 晶化过程 ; 核化 ; 结晶温度</subject><ispartof>International journal of minerals, metallurgy and materials, 2015-12, Vol.22 (12), p.1342-1349</ispartof><rights>University of Science and Technology Beijing and Springer-Verlag Berlin Heidelberg 2015</rights><rights>University of Science and Technology Beijing and Springer-Verlag Berlin Heidelberg 2015.</rights><rights>Copyright © Wanfang Data Co. 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Tailing-based glass samples were prepared fi'om Shandong gold tailings and Guyang iron tailings utilizing a conventional glass melting technique. For comparison, the tailing-based glass samples were crystallized using two different heat-treatment methods: conventional heating and hybrid microwave heating. The nucleation and crystallization temperatures were determined by performing a differential thermal analysis of the quenched tailing-based glass. The prepared glass-ceramic samples were further characterized by Fourier transform infrared spectroscopy, X-ray diffraction, Raman spectroscopy, thermal expansion coefficient measurements, and scanning electron microscopy. The results demonstrated that hybrid microwave heating could be successfully used to crystallize the tailing-based glass, reduce the processing time, and decrease the crystallization temperature. 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Tailing-based glass samples were prepared fi'om Shandong gold tailings and Guyang iron tailings utilizing a conventional glass melting technique. For comparison, the tailing-based glass samples were crystallized using two different heat-treatment methods: conventional heating and hybrid microwave heating. The nucleation and crystallization temperatures were determined by performing a differential thermal analysis of the quenched tailing-based glass. The prepared glass-ceramic samples were further characterized by Fourier transform infrared spectroscopy, X-ray diffraction, Raman spectroscopy, thermal expansion coefficient measurements, and scanning electron microscopy. The results demonstrated that hybrid microwave heating could be successfully used to crystallize the tailing-based glass, reduce the processing time, and decrease the crystallization temperature. Furthermore, the results indicated that the nucleation and crystallization mechanism of the hybrid microwave heating process slightly differs fi'om that of the conventional heating process.</abstract><cop>Beijing</cop><pub>University of Science and Technology Beijing</pub><doi>10.1007/s12613-015-1203-y</doi><tpages>8</tpages></addata></record>
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identifier ISSN: 1674-4799
ispartof International journal of minerals, metallurgy and materials, 2015-12, Vol.22 (12), p.1342-1349
issn 1674-4799
1869-103X
language eng
recordid cdi_wanfang_journals_bjkjdxxb_e201512014
source Springer Nature
subjects Ceramics
Characterization and Evaluation of Materials
Chemistry and Materials Science
Composites
Corrosion and Coatings
Crystallization
Differential thermal analysis
Fourier transforms
Glass
Glass ceramics
Heat treatment
Heating
Infrared spectroscopy
Materials Science
Metallic Materials
Microwave heating
Microwave radiation
Microwaves
Mine tailings
Natural Materials
Nucleation
Raman spectroscopy
Spectrum analysis
Surfaces and Interfaces
Tailings
Thermal analysis
Thermal expansion
Thin Films
Tribology
X-ray diffraction
X射线衍射仪
傅里叶变换红外光谱
尾矿微晶玻璃
微波加热
扫描电子显微镜
晶化过程
核化
结晶温度
title Nucleation and crystallization of tailing-based glass-ceramics by microwave heating
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