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Evaluation of depth of dislocation visibility in SEM electron channeling contrast imaging in Ti-6Al-4V alloy using serial sectioning method
Abstract In this study, we conducted a quantitative evaluation of dislocation density by scanning electron microscopy electron channeling contrast imaging for α grains of a Ti-6Al-4V alloy deformed at room temperature. The depth of visibility of dislocations is experimentally measured as 140 to 160...
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Published in: | Microscopy 2021-06, Vol.70 (3), p.265-277 |
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creator | Yamasaki, Shigeto Deguchi, Misaki Mitsuhara, Masatoshi Nakashima, Hideharu Ota, Yutaro Kubushiro, Keiji |
description | Abstract
In this study, we conducted a quantitative evaluation of dislocation density by scanning electron microscopy electron channeling contrast imaging for α grains of a Ti-6Al-4V alloy deformed at room temperature. The depth of visibility of dislocations is experimentally measured as 140 to 160 nm by a serial sectioning observation. This result is compared with the theoretical value and applied to evaluate dislocation density. These factors confirm that the theoretically calculated value of the depth of visibility, at 5 to 6 times the extinction distance, is valid for the hexagonal close-packed Ti alloy. |
doi_str_mv | 10.1093/jmicro/dfaa060 |
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In this study, we conducted a quantitative evaluation of dislocation density by scanning electron microscopy electron channeling contrast imaging for α grains of a Ti-6Al-4V alloy deformed at room temperature. The depth of visibility of dislocations is experimentally measured as 140 to 160 nm by a serial sectioning observation. This result is compared with the theoretical value and applied to evaluate dislocation density. These factors confirm that the theoretically calculated value of the depth of visibility, at 5 to 6 times the extinction distance, is valid for the hexagonal close-packed Ti alloy.</description><identifier>ISSN: 2050-5698</identifier><identifier>EISSN: 2050-5701</identifier><identifier>DOI: 10.1093/jmicro/dfaa060</identifier><language>eng</language><publisher>UK: Oxford University Press</publisher><ispartof>Microscopy, 2021-06, Vol.70 (3), p.265-277</ispartof><rights>The Author(s) 2020. Published by Oxford University Press on behalf of The Japanese Society of Microscopy. All rights reserved. For permissions, please e-mail: journals.permissions@oup.com 2020</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><cites>FETCH-LOGICAL-c261t-6b1072b9f6b241c94bfb1992fff6dc806b4cfaa513eb50c355b904b1f4dad7b33</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>315,786,790,1591,27957,27958</link.rule.ids></links><search><creatorcontrib>Yamasaki, Shigeto</creatorcontrib><creatorcontrib>Deguchi, Misaki</creatorcontrib><creatorcontrib>Mitsuhara, Masatoshi</creatorcontrib><creatorcontrib>Nakashima, Hideharu</creatorcontrib><creatorcontrib>Ota, Yutaro</creatorcontrib><creatorcontrib>Kubushiro, Keiji</creatorcontrib><title>Evaluation of depth of dislocation visibility in SEM electron channeling contrast imaging in Ti-6Al-4V alloy using serial sectioning method</title><title>Microscopy</title><description>Abstract
In this study, we conducted a quantitative evaluation of dislocation density by scanning electron microscopy electron channeling contrast imaging for α grains of a Ti-6Al-4V alloy deformed at room temperature. The depth of visibility of dislocations is experimentally measured as 140 to 160 nm by a serial sectioning observation. This result is compared with the theoretical value and applied to evaluate dislocation density. These factors confirm that the theoretically calculated value of the depth of visibility, at 5 to 6 times the extinction distance, is valid for the hexagonal close-packed Ti alloy.</description><issn>2050-5698</issn><issn>2050-5701</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2021</creationdate><recordtype>article</recordtype><recordid>eNqFkD1PwzAQhi0EElXpyuwRhlA7cdxkrKryIRUxUFgj27FbV04cbKdSfwN_GoeUmVvu9N57d7oHgFuMHjAqs_mh0cLZea0YQxRdgEmKcpTkC4Qv_2paFtdg5v0BxShyjAidgO_1kZmeBW1baBWsZRf2v4X2xopRP2qvuTY6nKBu4fv6FUojRXCxJfasbaXR7Q4K2wbHfIC6YbtBiN6tTujSJOQTMmPsCfZ-aHjpNDMxiWH9oDQy7G19A64UM17OznkKPh7X29Vzsnl7elktN4lIKQ4J5RgtUl4qylOCRUm44rgsU6UUrUWBKCciYshxJnmORJbnvESEY0VqVi94lk3B3bi3c_arlz5UjfZCGsNaaXtfpYQUJN7ARbQ-jNYI13snVdW5-J87VRhVA_hqBF-dwceB-3HA9t1_3h9M5omQ</recordid><startdate>20210606</startdate><enddate>20210606</enddate><creator>Yamasaki, Shigeto</creator><creator>Deguchi, Misaki</creator><creator>Mitsuhara, Masatoshi</creator><creator>Nakashima, Hideharu</creator><creator>Ota, Yutaro</creator><creator>Kubushiro, Keiji</creator><general>Oxford University Press</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope></search><sort><creationdate>20210606</creationdate><title>Evaluation of depth of dislocation visibility in SEM electron channeling contrast imaging in Ti-6Al-4V alloy using serial sectioning method</title><author>Yamasaki, Shigeto ; Deguchi, Misaki ; Mitsuhara, Masatoshi ; Nakashima, Hideharu ; Ota, Yutaro ; Kubushiro, Keiji</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c261t-6b1072b9f6b241c94bfb1992fff6dc806b4cfaa513eb50c355b904b1f4dad7b33</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2021</creationdate><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Yamasaki, Shigeto</creatorcontrib><creatorcontrib>Deguchi, Misaki</creatorcontrib><creatorcontrib>Mitsuhara, Masatoshi</creatorcontrib><creatorcontrib>Nakashima, Hideharu</creatorcontrib><creatorcontrib>Ota, Yutaro</creatorcontrib><creatorcontrib>Kubushiro, Keiji</creatorcontrib><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><jtitle>Microscopy</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Yamasaki, Shigeto</au><au>Deguchi, Misaki</au><au>Mitsuhara, Masatoshi</au><au>Nakashima, Hideharu</au><au>Ota, Yutaro</au><au>Kubushiro, Keiji</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Evaluation of depth of dislocation visibility in SEM electron channeling contrast imaging in Ti-6Al-4V alloy using serial sectioning method</atitle><jtitle>Microscopy</jtitle><date>2021-06-06</date><risdate>2021</risdate><volume>70</volume><issue>3</issue><spage>265</spage><epage>277</epage><pages>265-277</pages><issn>2050-5698</issn><eissn>2050-5701</eissn><notes>ObjectType-Article-1</notes><notes>SourceType-Scholarly Journals-1</notes><notes>ObjectType-Feature-2</notes><notes>content type line 23</notes><abstract>Abstract
In this study, we conducted a quantitative evaluation of dislocation density by scanning electron microscopy electron channeling contrast imaging for α grains of a Ti-6Al-4V alloy deformed at room temperature. The depth of visibility of dislocations is experimentally measured as 140 to 160 nm by a serial sectioning observation. This result is compared with the theoretical value and applied to evaluate dislocation density. These factors confirm that the theoretically calculated value of the depth of visibility, at 5 to 6 times the extinction distance, is valid for the hexagonal close-packed Ti alloy.</abstract><cop>UK</cop><pub>Oxford University Press</pub><doi>10.1093/jmicro/dfaa060</doi><tpages>13</tpages></addata></record> |
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title | Evaluation of depth of dislocation visibility in SEM electron channeling contrast imaging in Ti-6Al-4V alloy using serial sectioning method |
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