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Effect of Sn content on microstructure and boron distribution in Si–Al alloy
•Si–Al alloy with Sn addition was used for boron removal.•Sn addition effects on the eutectic silicon morphologies of Si–Al.•B was detected in Sn in much higher concentration than in Al by EPMA line analysis. Si–Al and Si–Al–Sn alloy melts were used for silicon purification by alloy solidification r...
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Published in: | Journal of alloys and compounds 2014, Vol.583, p.85-90 |
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creator | Li, Yaqiong Tan, Yi Li, Jiayan Xu, Qiang Liu, Yao |
description | •Si–Al alloy with Sn addition was used for boron removal.•Sn addition effects on the eutectic silicon morphologies of Si–Al.•B was detected in Sn in much higher concentration than in Al by EPMA line analysis.
Si–Al and Si–Al–Sn alloy melts were used for silicon purification by alloy solidification refining method. The effects of Sn addition on alloy microstructure, eutectic Si morphology, as well as B distribution were investigated using optical microscopy, scanning electron microscopy, electron probe microanalyzer and inductively coupled plasma mass spectrometer. Primary Si and αAl+Si structures with flake-like eutectic Si were found in Si–Al alloy; while an additional structure of αAl+βSn+Si in Si–Al–Sn alloy was found. Si in αAl+Si eutectic had a globular shape, whereas some Si in αAl+βSn+Si eutectic had an octahedral shape. Compared with primary Si, more boron was found to distribute in final solidified phase during the solidification, i.e. αAl+Si for Si–Al system and αAl+βSn+Si for Si–Al–Sn system. The refining ratio of B decreased with increasing Al content in Si–Al alloy melt, while increased with Sn addition using Si–Al–Sn alloy melt. |
doi_str_mv | 10.1016/j.jallcom.2013.08.145 |
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Si–Al and Si–Al–Sn alloy melts were used for silicon purification by alloy solidification refining method. The effects of Sn addition on alloy microstructure, eutectic Si morphology, as well as B distribution were investigated using optical microscopy, scanning electron microscopy, electron probe microanalyzer and inductively coupled plasma mass spectrometer. Primary Si and αAl+Si structures with flake-like eutectic Si were found in Si–Al alloy; while an additional structure of αAl+βSn+Si in Si–Al–Sn alloy was found. Si in αAl+Si eutectic had a globular shape, whereas some Si in αAl+βSn+Si eutectic had an octahedral shape. Compared with primary Si, more boron was found to distribute in final solidified phase during the solidification, i.e. αAl+Si for Si–Al system and αAl+βSn+Si for Si–Al–Sn system. The refining ratio of B decreased with increasing Al content in Si–Al alloy melt, while increased with Sn addition using Si–Al–Sn alloy melt.</description><identifier>ISSN: 0925-8388</identifier><identifier>EISSN: 1873-4669</identifier><identifier>DOI: 10.1016/j.jallcom.2013.08.145</identifier><language>eng</language><publisher>Kidlington: Elsevier B.V</publisher><subject>Alloy solidification refining method ; Alloying additive ; Boron ; Boron distribution ; Cross-disciplinary physics: materials science; rheology ; Eutectics ; Exact sciences and technology ; Materials science ; Melts ; Microstructure ; Microstructure and morphology ; Phase diagrams and microstructures developed by solidification and solid-solid phase transformations ; Physics ; Refining ; Silicon ; Si–Al alloy ; Solidification ; Tin</subject><ispartof>Journal of alloys and compounds, 2014, Vol.583, p.85-90</ispartof><rights>2013 Elsevier B.V.</rights><rights>2015 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c438t-67ff8f776a766be11a192627d21fa8e70514f27063b7ab8f874fb2184d833bb53</citedby><cites>FETCH-LOGICAL-c438t-67ff8f776a766be11a192627d21fa8e70514f27063b7ab8f874fb2184d833bb53</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>315,786,790,4043,27956,27957,27958</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=28259148$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Li, Yaqiong</creatorcontrib><creatorcontrib>Tan, Yi</creatorcontrib><creatorcontrib>Li, Jiayan</creatorcontrib><creatorcontrib>Xu, Qiang</creatorcontrib><creatorcontrib>Liu, Yao</creatorcontrib><title>Effect of Sn content on microstructure and boron distribution in Si–Al alloy</title><title>Journal of alloys and compounds</title><description>•Si–Al alloy with Sn addition was used for boron removal.•Sn addition effects on the eutectic silicon morphologies of Si–Al.•B was detected in Sn in much higher concentration than in Al by EPMA line analysis.
Si–Al and Si–Al–Sn alloy melts were used for silicon purification by alloy solidification refining method. The effects of Sn addition on alloy microstructure, eutectic Si morphology, as well as B distribution were investigated using optical microscopy, scanning electron microscopy, electron probe microanalyzer and inductively coupled plasma mass spectrometer. Primary Si and αAl+Si structures with flake-like eutectic Si were found in Si–Al alloy; while an additional structure of αAl+βSn+Si in Si–Al–Sn alloy was found. Si in αAl+Si eutectic had a globular shape, whereas some Si in αAl+βSn+Si eutectic had an octahedral shape. Compared with primary Si, more boron was found to distribute in final solidified phase during the solidification, i.e. αAl+Si for Si–Al system and αAl+βSn+Si for Si–Al–Sn system. The refining ratio of B decreased with increasing Al content in Si–Al alloy melt, while increased with Sn addition using Si–Al–Sn alloy melt.</description><subject>Alloy solidification refining method</subject><subject>Alloying additive</subject><subject>Boron</subject><subject>Boron distribution</subject><subject>Cross-disciplinary physics: materials science; rheology</subject><subject>Eutectics</subject><subject>Exact sciences and technology</subject><subject>Materials science</subject><subject>Melts</subject><subject>Microstructure</subject><subject>Microstructure and morphology</subject><subject>Phase diagrams and microstructures developed by solidification and solid-solid phase transformations</subject><subject>Physics</subject><subject>Refining</subject><subject>Silicon</subject><subject>Si–Al alloy</subject><subject>Solidification</subject><subject>Tin</subject><issn>0925-8388</issn><issn>1873-4669</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2014</creationdate><recordtype>article</recordtype><recordid>eNqFkM1KxDAQx4MouH48gtCL4KU1k7RJehJZ_ALRw-o5pGkCWbrJmrTC3nwH39AnMcsuXj0NM_Of-c_8ELoAXAEGdr2slmoYdFhVBAOtsKigbg7QDASnZc1Ye4hmuCVNKagQx-gkpSXGGFoKM_RyZ63RYxFssfCFDn40Pme-WDkdQxrjpMcpmkL5vuhCzI3e5arrptHlxPli4X6-vm-HIp8QNmfoyKohmfN9PEXv93dv88fy-fXhaX77XOqairFk3FphOWeKM9YZAAUtYYT3BKwShuMGaks4ZrTjqhNW8Np2BETdC0q7rqGn6Gq3dx3Dx2TSKFcuaTMMypswJQmMA8OCYpqlzU66_SdFY-U6upWKGwlYbvnJpdzzk1t-EguZ-eW5y72FSloNNiqvXfobJoI0LdQi6252OpP__XQmyqSd8dr0Lmaysg_uH6dfEsGJKA</recordid><startdate>2014</startdate><enddate>2014</enddate><creator>Li, Yaqiong</creator><creator>Tan, Yi</creator><creator>Li, Jiayan</creator><creator>Xu, Qiang</creator><creator>Liu, Yao</creator><general>Elsevier B.V</general><general>Elsevier</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7QF</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>2014</creationdate><title>Effect of Sn content on microstructure and boron distribution in Si–Al alloy</title><author>Li, Yaqiong ; Tan, Yi ; Li, Jiayan ; Xu, Qiang ; Liu, Yao</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c438t-67ff8f776a766be11a192627d21fa8e70514f27063b7ab8f874fb2184d833bb53</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2014</creationdate><topic>Alloy solidification refining method</topic><topic>Alloying additive</topic><topic>Boron</topic><topic>Boron distribution</topic><topic>Cross-disciplinary physics: materials science; rheology</topic><topic>Eutectics</topic><topic>Exact sciences and technology</topic><topic>Materials science</topic><topic>Melts</topic><topic>Microstructure</topic><topic>Microstructure and morphology</topic><topic>Phase diagrams and microstructures developed by solidification and solid-solid phase transformations</topic><topic>Physics</topic><topic>Refining</topic><topic>Silicon</topic><topic>Si–Al alloy</topic><topic>Solidification</topic><topic>Tin</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Li, Yaqiong</creatorcontrib><creatorcontrib>Tan, Yi</creatorcontrib><creatorcontrib>Li, Jiayan</creatorcontrib><creatorcontrib>Xu, Qiang</creatorcontrib><creatorcontrib>Liu, Yao</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>Aluminium Industry Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Journal of alloys and compounds</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Li, Yaqiong</au><au>Tan, Yi</au><au>Li, Jiayan</au><au>Xu, Qiang</au><au>Liu, Yao</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Effect of Sn content on microstructure and boron distribution in Si–Al alloy</atitle><jtitle>Journal of alloys and compounds</jtitle><date>2014</date><risdate>2014</risdate><volume>583</volume><spage>85</spage><epage>90</epage><pages>85-90</pages><issn>0925-8388</issn><eissn>1873-4669</eissn><notes>ObjectType-Article-1</notes><notes>SourceType-Scholarly Journals-1</notes><notes>ObjectType-Feature-2</notes><notes>content type line 23</notes><abstract>•Si–Al alloy with Sn addition was used for boron removal.•Sn addition effects on the eutectic silicon morphologies of Si–Al.•B was detected in Sn in much higher concentration than in Al by EPMA line analysis.
Si–Al and Si–Al–Sn alloy melts were used for silicon purification by alloy solidification refining method. The effects of Sn addition on alloy microstructure, eutectic Si morphology, as well as B distribution were investigated using optical microscopy, scanning electron microscopy, electron probe microanalyzer and inductively coupled plasma mass spectrometer. Primary Si and αAl+Si structures with flake-like eutectic Si were found in Si–Al alloy; while an additional structure of αAl+βSn+Si in Si–Al–Sn alloy was found. Si in αAl+Si eutectic had a globular shape, whereas some Si in αAl+βSn+Si eutectic had an octahedral shape. Compared with primary Si, more boron was found to distribute in final solidified phase during the solidification, i.e. αAl+Si for Si–Al system and αAl+βSn+Si for Si–Al–Sn system. The refining ratio of B decreased with increasing Al content in Si–Al alloy melt, while increased with Sn addition using Si–Al–Sn alloy melt.</abstract><cop>Kidlington</cop><pub>Elsevier B.V</pub><doi>10.1016/j.jallcom.2013.08.145</doi><tpages>6</tpages></addata></record> |
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subjects | Alloy solidification refining method Alloying additive Boron Boron distribution Cross-disciplinary physics: materials science rheology Eutectics Exact sciences and technology Materials science Melts Microstructure Microstructure and morphology Phase diagrams and microstructures developed by solidification and solid-solid phase transformations Physics Refining Silicon Si–Al alloy Solidification Tin |
title | Effect of Sn content on microstructure and boron distribution in Si–Al alloy |
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