Loading…
DSC estimation of structural and textural parameters of SBA-15 silica using water probe
The aim of this study was to use DSC and X-ray diffraction measurements to determine the pore size and pore wall thickness of highly ordered SBA-15 materials. The DSC curves showed two endothermic events during the heating cycle. These events were due to the presence of water inside and outside of m...
Saved in:
| Published in: | Journal of thermal analysis and calorimetry 2009-08, Vol.97 (2), p.701-704 |
|---|---|
| Main Authors: | , , , , , , , |
| Format: | Article |
| Language: | English |
| Subjects: | |
| Citations: | Items that this one cites Items that cite this one |
| Online Access: | Get full text |
| Tags: |
Add Tag
No Tags, Be the first to tag this record!
|
| cited_by | cdi_FETCH-LOGICAL-c351t-96f1630a2e14a81e582ff3a530309336d3c09f861812238c1b9650c38f60b6ce3 |
|---|---|
| cites | cdi_FETCH-LOGICAL-c351t-96f1630a2e14a81e582ff3a530309336d3c09f861812238c1b9650c38f60b6ce3 |
| container_end_page | 704 |
| container_issue | 2 |
| container_start_page | 701 |
| container_title | Journal of thermal analysis and calorimetry |
| container_volume | 97 |
| creator | Cides da Silva, L. C. Araújo, G. L. B. Segismundo, N. R. Moscardini, E. F. Mercuri, L. P. Cosentino, I. C. Fantini, M. C. A. Matos, J. R. |
| description | The aim of this study was to use DSC and X-ray diffraction measurements to determine the pore size and pore wall thickness of highly ordered SBA-15 materials. The DSC curves showed two endothermic events during the heating cycle. These events were due to the presence of water inside and outside of mesopores. The results of pore radius, wall thickness and pore volume measurements were in good agreement with the results obtained by nitrogen adsorption measurement, XRD and transmission electron microscopy. |
| doi_str_mv | 10.1007/s10973-009-0334-7 |
| format | article |
| fullrecord | <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_miscellaneous_1671260495</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>1671260495</sourcerecordid><originalsourceid>FETCH-LOGICAL-c351t-96f1630a2e14a81e582ff3a530309336d3c09f861812238c1b9650c38f60b6ce3</originalsourceid><addsrcrecordid>eNp9kE9LAzEQxYMoWLQfwFsugpfVmWSTTY61_oWChyoeQ5omZWW7W5Nd1G9vyhaPnmaG-c0b3iPkAuEaAaqbhKArXgDoAjgvi-qITFAoVTDN5HHuee4lCjgl05TqFTAEqYXSE_J-t5xTn_p6a_u6a2kXaOrj4Poh2obadk17_z0OOxvt1vc-pj21vJ0VKGiqm9pZOqS63dAvm7d0F7uVPycnwTbJTw_1jLw93L_On4rFy-PzfLYoHBfYF1oGlBws81hahV4oFgK3ggMHzblccwc6KIkKGePK4UpLAY6rIGElnedn5GrUzV8_h2zEbOvkfNPY1ndDMigrZBJKLTKKI-pil1L0wexith1_DILZ52jGHE3O0exzNFW-uTzI2-RsE6JtXZ3-DhmDSohSZ46NXMqrduOj-eiG2Gbn_4j_AgKrgJk</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>1671260495</pqid></control><display><type>article</type><title>DSC estimation of structural and textural parameters of SBA-15 silica using water probe</title><source>Springer Link</source><creator>Cides da Silva, L. C. ; Araújo, G. L. B. ; Segismundo, N. R. ; Moscardini, E. F. ; Mercuri, L. P. ; Cosentino, I. C. ; Fantini, M. C. A. ; Matos, J. R.</creator><creatorcontrib>Cides da Silva, L. C. ; Araújo, G. L. B. ; Segismundo, N. R. ; Moscardini, E. F. ; Mercuri, L. P. ; Cosentino, I. C. ; Fantini, M. C. A. ; Matos, J. R.</creatorcontrib><description>The aim of this study was to use DSC and X-ray diffraction measurements to determine the pore size and pore wall thickness of highly ordered SBA-15 materials. The DSC curves showed two endothermic events during the heating cycle. These events were due to the presence of water inside and outside of mesopores. The results of pore radius, wall thickness and pore volume measurements were in good agreement with the results obtained by nitrogen adsorption measurement, XRD and transmission electron microscopy.</description><identifier>ISSN: 1388-6150</identifier><identifier>EISSN: 1588-2926</identifier><identifier>EISSN: 1572-8943</identifier><identifier>DOI: 10.1007/s10973-009-0334-7</identifier><language>eng</language><publisher>Dordrecht: Springer Netherlands</publisher><subject>Analytical Chemistry ; Calorimetry ; Chemistry ; Chemistry and Materials Science ; Colloidal state and disperse state ; Differential scanning calorimetry ; Diffraction ; Endothermic reactions ; Exact sciences and technology ; General and physical chemistry ; Heating ; Inorganic Chemistry ; Measurement Science and Instrumentation ; Physical Chemistry ; Polymer Sciences ; Porosity ; Porous materials ; Wall thickness ; X-rays</subject><ispartof>Journal of thermal analysis and calorimetry, 2009-08, Vol.97 (2), p.701-704</ispartof><rights>Akadémiai Kiadó, Budapest, Hungary 2009</rights><rights>2015 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c351t-96f1630a2e14a81e582ff3a530309336d3c09f861812238c1b9650c38f60b6ce3</citedby><cites>FETCH-LOGICAL-c351t-96f1630a2e14a81e582ff3a530309336d3c09f861812238c1b9650c38f60b6ce3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>315,786,790,27957,27958</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=22075549$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Cides da Silva, L. C.</creatorcontrib><creatorcontrib>Araújo, G. L. B.</creatorcontrib><creatorcontrib>Segismundo, N. R.</creatorcontrib><creatorcontrib>Moscardini, E. F.</creatorcontrib><creatorcontrib>Mercuri, L. P.</creatorcontrib><creatorcontrib>Cosentino, I. C.</creatorcontrib><creatorcontrib>Fantini, M. C. A.</creatorcontrib><creatorcontrib>Matos, J. R.</creatorcontrib><title>DSC estimation of structural and textural parameters of SBA-15 silica using water probe</title><title>Journal of thermal analysis and calorimetry</title><addtitle>J Therm Anal Calorim</addtitle><description>The aim of this study was to use DSC and X-ray diffraction measurements to determine the pore size and pore wall thickness of highly ordered SBA-15 materials. The DSC curves showed two endothermic events during the heating cycle. These events were due to the presence of water inside and outside of mesopores. The results of pore radius, wall thickness and pore volume measurements were in good agreement with the results obtained by nitrogen adsorption measurement, XRD and transmission electron microscopy.</description><subject>Analytical Chemistry</subject><subject>Calorimetry</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Colloidal state and disperse state</subject><subject>Differential scanning calorimetry</subject><subject>Diffraction</subject><subject>Endothermic reactions</subject><subject>Exact sciences and technology</subject><subject>General and physical chemistry</subject><subject>Heating</subject><subject>Inorganic Chemistry</subject><subject>Measurement Science and Instrumentation</subject><subject>Physical Chemistry</subject><subject>Polymer Sciences</subject><subject>Porosity</subject><subject>Porous materials</subject><subject>Wall thickness</subject><subject>X-rays</subject><issn>1388-6150</issn><issn>1588-2926</issn><issn>1572-8943</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2009</creationdate><recordtype>article</recordtype><recordid>eNp9kE9LAzEQxYMoWLQfwFsugpfVmWSTTY61_oWChyoeQ5omZWW7W5Nd1G9vyhaPnmaG-c0b3iPkAuEaAaqbhKArXgDoAjgvi-qITFAoVTDN5HHuee4lCjgl05TqFTAEqYXSE_J-t5xTn_p6a_u6a2kXaOrj4Poh2obadk17_z0OOxvt1vc-pj21vJ0VKGiqm9pZOqS63dAvm7d0F7uVPycnwTbJTw_1jLw93L_On4rFy-PzfLYoHBfYF1oGlBws81hahV4oFgK3ggMHzblccwc6KIkKGePK4UpLAY6rIGElnedn5GrUzV8_h2zEbOvkfNPY1ndDMigrZBJKLTKKI-pil1L0wexith1_DILZ52jGHE3O0exzNFW-uTzI2-RsE6JtXZ3-DhmDSohSZ46NXMqrduOj-eiG2Gbn_4j_AgKrgJk</recordid><startdate>20090801</startdate><enddate>20090801</enddate><creator>Cides da Silva, L. C.</creator><creator>Araújo, G. L. B.</creator><creator>Segismundo, N. R.</creator><creator>Moscardini, E. F.</creator><creator>Mercuri, L. P.</creator><creator>Cosentino, I. C.</creator><creator>Fantini, M. C. A.</creator><creator>Matos, J. R.</creator><general>Springer Netherlands</general><general>Springer</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><scope>L7M</scope></search><sort><creationdate>20090801</creationdate><title>DSC estimation of structural and textural parameters of SBA-15 silica using water probe</title><author>Cides da Silva, L. C. ; Araújo, G. L. B. ; Segismundo, N. R. ; Moscardini, E. F. ; Mercuri, L. P. ; Cosentino, I. C. ; Fantini, M. C. A. ; Matos, J. R.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c351t-96f1630a2e14a81e582ff3a530309336d3c09f861812238c1b9650c38f60b6ce3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2009</creationdate><topic>Analytical Chemistry</topic><topic>Calorimetry</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Colloidal state and disperse state</topic><topic>Differential scanning calorimetry</topic><topic>Diffraction</topic><topic>Endothermic reactions</topic><topic>Exact sciences and technology</topic><topic>General and physical chemistry</topic><topic>Heating</topic><topic>Inorganic Chemistry</topic><topic>Measurement Science and Instrumentation</topic><topic>Physical Chemistry</topic><topic>Polymer Sciences</topic><topic>Porosity</topic><topic>Porous materials</topic><topic>Wall thickness</topic><topic>X-rays</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Cides da Silva, L. C.</creatorcontrib><creatorcontrib>Araújo, G. L. B.</creatorcontrib><creatorcontrib>Segismundo, N. R.</creatorcontrib><creatorcontrib>Moscardini, E. F.</creatorcontrib><creatorcontrib>Mercuri, L. P.</creatorcontrib><creatorcontrib>Cosentino, I. C.</creatorcontrib><creatorcontrib>Fantini, M. C. A.</creatorcontrib><creatorcontrib>Matos, J. R.</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Journal of thermal analysis and calorimetry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Cides da Silva, L. C.</au><au>Araújo, G. L. B.</au><au>Segismundo, N. R.</au><au>Moscardini, E. F.</au><au>Mercuri, L. P.</au><au>Cosentino, I. C.</au><au>Fantini, M. C. A.</au><au>Matos, J. R.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>DSC estimation of structural and textural parameters of SBA-15 silica using water probe</atitle><jtitle>Journal of thermal analysis and calorimetry</jtitle><stitle>J Therm Anal Calorim</stitle><date>2009-08-01</date><risdate>2009</risdate><volume>97</volume><issue>2</issue><spage>701</spage><epage>704</epage><pages>701-704</pages><issn>1388-6150</issn><eissn>1588-2926</eissn><eissn>1572-8943</eissn><notes>ObjectType-Article-1</notes><notes>SourceType-Scholarly Journals-1</notes><notes>ObjectType-Feature-2</notes><notes>content type line 23</notes><abstract>The aim of this study was to use DSC and X-ray diffraction measurements to determine the pore size and pore wall thickness of highly ordered SBA-15 materials. The DSC curves showed two endothermic events during the heating cycle. These events were due to the presence of water inside and outside of mesopores. The results of pore radius, wall thickness and pore volume measurements were in good agreement with the results obtained by nitrogen adsorption measurement, XRD and transmission electron microscopy.</abstract><cop>Dordrecht</cop><pub>Springer Netherlands</pub><doi>10.1007/s10973-009-0334-7</doi><tpages>4</tpages></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 1388-6150 |
| ispartof | Journal of thermal analysis and calorimetry, 2009-08, Vol.97 (2), p.701-704 |
| issn | 1388-6150 1588-2926 1572-8943 |
| language | eng |
| recordid | cdi_proquest_miscellaneous_1671260495 |
| source | Springer Link |
| subjects | Analytical Chemistry Calorimetry Chemistry Chemistry and Materials Science Colloidal state and disperse state Differential scanning calorimetry Diffraction Endothermic reactions Exact sciences and technology General and physical chemistry Heating Inorganic Chemistry Measurement Science and Instrumentation Physical Chemistry Polymer Sciences Porosity Porous materials Wall thickness X-rays |
| title | DSC estimation of structural and textural parameters of SBA-15 silica using water probe |
| url | http://sfxeu10.hosted.exlibrisgroup.com/loughborough?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2024-09-22T06%3A43%3A35IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=DSC%20estimation%20of%20structural%20and%20textural%20parameters%20of%20SBA-15%20silica%20using%20water%20probe&rft.jtitle=Journal%20of%20thermal%20analysis%20and%20calorimetry&rft.au=Cides%20da%20Silva,%20L.%20C.&rft.date=2009-08-01&rft.volume=97&rft.issue=2&rft.spage=701&rft.epage=704&rft.pages=701-704&rft.issn=1388-6150&rft.eissn=1588-2926&rft_id=info:doi/10.1007/s10973-009-0334-7&rft_dat=%3Cproquest_cross%3E1671260495%3C/proquest_cross%3E%3Cgrp_id%3Ecdi_FETCH-LOGICAL-c351t-96f1630a2e14a81e582ff3a530309336d3c09f861812238c1b9650c38f60b6ce3%3C/grp_id%3E%3Coa%3E%3C/oa%3E%3Curl%3E%3C/url%3E&rft_id=info:oai/&rft_pqid=1671260495&rft_id=info:pmid/&rfr_iscdi=true |