An efficient catalyst-free and chemoselective synthesis of azobenzenes from nitrobenzenes

NaOH mediated reaction of nitrobenzenes in EtOH was performed at 80 degree C temperature affording azobenzenes in excellent yield. This methodology presents an easy synthesis of a wide variety of azo compounds from readily available nitrobenzene derivatives.

Saved in:
Bibliographic Details
Published in:RSC advances 2014-01, Vol.4 (81), p.42947-42951
Main Authors: Gund, Sitaram H., Shelkar, Radheshyam S., Nagarkar, Jayashree M.
Format: Article
Language:English
Subjects:
Azo compounds
Catalysts
Derivatives
Methodology
Nitrobenzenes
Synthesis
Citations: Items that this one cites
Items that cite this one
Online Access:Get full text
Tags: Add Tag
No Tags, Be the first to tag this record!
cited_by cdi_FETCH-LOGICAL-c330t-3ba8949ab7d9a16b3a3daf5e29a1f160aed39c656c68201bb52391ea0a2c5a913
cites cdi_FETCH-LOGICAL-c330t-3ba8949ab7d9a16b3a3daf5e29a1f160aed39c656c68201bb52391ea0a2c5a913
container_end_page 42951
container_issue 81
container_start_page 42947
container_title RSC advances
container_volume 4
creator Gund, Sitaram H.
Shelkar, Radheshyam S.
Nagarkar, Jayashree M.
description NaOH mediated reaction of nitrobenzenes in EtOH was performed at 80 degree C temperature affording azobenzenes in excellent yield. This methodology presents an easy synthesis of a wide variety of azo compounds from readily available nitrobenzene derivatives.
doi_str_mv 10.1039/C4RA06027J
format article
fullrecord <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_miscellaneous_1660081907</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>1660081907</sourcerecordid><originalsourceid>FETCH-LOGICAL-c330t-3ba8949ab7d9a16b3a3daf5e29a1f160aed39c656c68201bb52391ea0a2c5a913</originalsourceid><addsrcrecordid>eNpNUE1LAzEUDKJgqb34C3IUYfUl6abNsRQ_KQiiB0_L2-wLjexma5IK219vpaLOZT4Y5jCMnQu4EqDM9XL6vAANcvZ4xEYSprqQoM3xP33KJim9wx66FFKLEXtbBE7OeespZG4xYzukXLhIxDE03K6p6xO1ZLP_JJ6GkNeUfOK947jrawo7CpS4i33Hg8_xNzpjJw7bRJMfHrPX25uX5X2xerp7WC5WhVUKcqFqnJupwXrWGBS6VqgadCXJvXNCA1KjjNWltnouQdR1KZURhIDSlmiEGrOLw-4m9h9bSrnqfLLUthio36ZKaA0wFwZm--rloWpjn1IkV22i7zAOlYDq-8Lq70L1BZwlZLo</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>1660081907</pqid></control><display><type>article</type><title>An efficient catalyst-free and chemoselective synthesis of azobenzenes from nitrobenzenes</title><source>Royal Society of Chemistry:Jisc Collections:Royal Society of Chemistry Read and Publish 2022-2024 (reading list)</source><creator>Gund, Sitaram H. ; Shelkar, Radheshyam S. ; Nagarkar, Jayashree M.</creator><creatorcontrib>Gund, Sitaram H. ; Shelkar, Radheshyam S. ; Nagarkar, Jayashree M.</creatorcontrib><description>NaOH mediated reaction of nitrobenzenes in EtOH was performed at 80 degree C temperature affording azobenzenes in excellent yield. This methodology presents an easy synthesis of a wide variety of azo compounds from readily available nitrobenzene derivatives.</description><identifier>ISSN: 2046-2069</identifier><identifier>EISSN: 2046-2069</identifier><identifier>DOI: 10.1039/C4RA06027J</identifier><language>eng</language><subject>Azo compounds ; Catalysts ; Derivatives ; Methodology ; Nitrobenzenes ; Synthesis</subject><ispartof>RSC advances, 2014-01, Vol.4 (81), p.42947-42951</ispartof><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c330t-3ba8949ab7d9a16b3a3daf5e29a1f160aed39c656c68201bb52391ea0a2c5a913</citedby><cites>FETCH-LOGICAL-c330t-3ba8949ab7d9a16b3a3daf5e29a1f160aed39c656c68201bb52391ea0a2c5a913</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>315,786,790,27957,27958</link.rule.ids></links><search><creatorcontrib>Gund, Sitaram H.</creatorcontrib><creatorcontrib>Shelkar, Radheshyam S.</creatorcontrib><creatorcontrib>Nagarkar, Jayashree M.</creatorcontrib><title>An efficient catalyst-free and chemoselective synthesis of azobenzenes from nitrobenzenes</title><title>RSC advances</title><description>NaOH mediated reaction of nitrobenzenes in EtOH was performed at 80 degree C temperature affording azobenzenes in excellent yield. This methodology presents an easy synthesis of a wide variety of azo compounds from readily available nitrobenzene derivatives.</description><subject>Azo compounds</subject><subject>Catalysts</subject><subject>Derivatives</subject><subject>Methodology</subject><subject>Nitrobenzenes</subject><subject>Synthesis</subject><issn>2046-2069</issn><issn>2046-2069</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2014</creationdate><recordtype>article</recordtype><recordid>eNpNUE1LAzEUDKJgqb34C3IUYfUl6abNsRQ_KQiiB0_L2-wLjexma5IK219vpaLOZT4Y5jCMnQu4EqDM9XL6vAANcvZ4xEYSprqQoM3xP33KJim9wx66FFKLEXtbBE7OeespZG4xYzukXLhIxDE03K6p6xO1ZLP_JJ6GkNeUfOK947jrawo7CpS4i33Hg8_xNzpjJw7bRJMfHrPX25uX5X2xerp7WC5WhVUKcqFqnJupwXrWGBS6VqgadCXJvXNCA1KjjNWltnouQdR1KZURhIDSlmiEGrOLw-4m9h9bSrnqfLLUthio36ZKaA0wFwZm--rloWpjn1IkV22i7zAOlYDq-8Lq70L1BZwlZLo</recordid><startdate>20140101</startdate><enddate>20140101</enddate><creator>Gund, Sitaram H.</creator><creator>Shelkar, Radheshyam S.</creator><creator>Nagarkar, Jayashree M.</creator><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>20140101</creationdate><title>An efficient catalyst-free and chemoselective synthesis of azobenzenes from nitrobenzenes</title><author>Gund, Sitaram H. ; Shelkar, Radheshyam S. ; Nagarkar, Jayashree M.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c330t-3ba8949ab7d9a16b3a3daf5e29a1f160aed39c656c68201bb52391ea0a2c5a913</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2014</creationdate><topic>Azo compounds</topic><topic>Catalysts</topic><topic>Derivatives</topic><topic>Methodology</topic><topic>Nitrobenzenes</topic><topic>Synthesis</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Gund, Sitaram H.</creatorcontrib><creatorcontrib>Shelkar, Radheshyam S.</creatorcontrib><creatorcontrib>Nagarkar, Jayashree M.</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>RSC advances</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Gund, Sitaram H.</au><au>Shelkar, Radheshyam S.</au><au>Nagarkar, Jayashree M.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>An efficient catalyst-free and chemoselective synthesis of azobenzenes from nitrobenzenes</atitle><jtitle>RSC advances</jtitle><date>2014-01-01</date><risdate>2014</risdate><volume>4</volume><issue>81</issue><spage>42947</spage><epage>42951</epage><pages>42947-42951</pages><issn>2046-2069</issn><eissn>2046-2069</eissn><notes>ObjectType-Article-1</notes><notes>SourceType-Scholarly Journals-1</notes><notes>ObjectType-Feature-2</notes><notes>content type line 23</notes><abstract>NaOH mediated reaction of nitrobenzenes in EtOH was performed at 80 degree C temperature affording azobenzenes in excellent yield. This methodology presents an easy synthesis of a wide variety of azo compounds from readily available nitrobenzene derivatives.</abstract><doi>10.1039/C4RA06027J</doi><tpages>5</tpages></addata></record>
fulltext fulltext
identifier ISSN: 2046-2069
ispartof RSC advances, 2014-01, Vol.4 (81), p.42947-42951
issn 2046-2069
2046-2069
language eng
recordid cdi_proquest_miscellaneous_1660081907
source Royal Society of Chemistry:Jisc Collections:Royal Society of Chemistry Read and Publish 2022-2024 (reading list)
subjects Azo compounds
Catalysts
Derivatives
Methodology
Nitrobenzenes
Synthesis
title An efficient catalyst-free and chemoselective synthesis of azobenzenes from nitrobenzenes
url http://sfxeu10.hosted.exlibrisgroup.com/loughborough?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2024-09-23T00%3A14%3A13IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=An%20efficient%20catalyst-free%20and%20chemoselective%20synthesis%20of%20azobenzenes%20from%20nitrobenzenes&rft.jtitle=RSC%20advances&rft.au=Gund,%20Sitaram%20H.&rft.date=2014-01-01&rft.volume=4&rft.issue=81&rft.spage=42947&rft.epage=42951&rft.pages=42947-42951&rft.issn=2046-2069&rft.eissn=2046-2069&rft_id=info:doi/10.1039/C4RA06027J&rft_dat=%3Cproquest_cross%3E1660081907%3C/proquest_cross%3E%3Cgrp_id%3Ecdi_FETCH-LOGICAL-c330t-3ba8949ab7d9a16b3a3daf5e29a1f160aed39c656c68201bb52391ea0a2c5a913%3C/grp_id%3E%3Coa%3E%3C/oa%3E%3Curl%3E%3C/url%3E&rft_id=info:oai/&rft_pqid=1660081907&rft_id=info:pmid/&rfr_iscdi=true