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Urea-based synthesis of magnetite nanoparticles and its composite with graphene oxide: structural and magnetic characterization
Magnetite-loaded graphene oxide nanocomposites are currently studied as an easily retrievable efficient adsorbent of dyes and heavy metals. Therefore, the search for facile and low cost synthetical methods to prepare them is intensively pursued. This work describes a simple one-pot method to produce...
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| Published in: | Journal of materials science. Materials in electronics 2020-05, Vol.31 (10), p.7490-7498 |
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| Main Authors: | , , , |
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| cited_by | cdi_FETCH-LOGICAL-c319t-f58809072f3a48fffa326785928c82fb66bc8ffbb4ede9752cd863fc0bd97cb23 |
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| cites | cdi_FETCH-LOGICAL-c319t-f58809072f3a48fffa326785928c82fb66bc8ffbb4ede9752cd863fc0bd97cb23 |
| container_end_page | 7498 |
| container_issue | 10 |
| container_start_page | 7490 |
| container_title | Journal of materials science. Materials in electronics |
| container_volume | 31 |
| creator | Pérez-Guzmán, M. A. Ortega-Amaya, R. Santoyo-Salazar, J. Ortega-López, M. |
| description | Magnetite-loaded graphene oxide nanocomposites are currently studied as an easily retrievable efficient adsorbent of dyes and heavy metals. Therefore, the search for facile and low cost synthetical methods to prepare them is intensively pursued. This work describes a simple one-pot method to produce superparamagnetic magnetite nanoparticles (Fe
3
O
4
), and a hybrid nanocomposite of magnetite nanoparticles decorating reduced graphene oxide (Fe
3
O
4
–rGO) by reacting ferrous chloride with urea in water or graphene oxide–water dispersions, respectively. The synthetical method is based on temperature-assisted urea decomposition in water. The final products comprised Fe
3
O
4
nanoparticles or Fe
3
O
4
-decorated rGO sheets. Outstandingly, despite the polydisperse nature of Fe
3
O
4
, both materials are nearly superparamagnetic, and GO was partially reduced during the Fe
3
O
4
–GO preparation to produce Fe
3
O
4
–rGO. We propose plausible pathways for the Fe
3
O
4
formation, as well as a preliminary study on methylene blue degradation in water, using the Fe
3
O
4
–rGO nanocomposite. |
| doi_str_mv | 10.1007/s10854-020-02989-5 |
| format | article |
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3
O
4
), and a hybrid nanocomposite of magnetite nanoparticles decorating reduced graphene oxide (Fe
3
O
4
–rGO) by reacting ferrous chloride with urea in water or graphene oxide–water dispersions, respectively. The synthetical method is based on temperature-assisted urea decomposition in water. The final products comprised Fe
3
O
4
nanoparticles or Fe
3
O
4
-decorated rGO sheets. Outstandingly, despite the polydisperse nature of Fe
3
O
4
, both materials are nearly superparamagnetic, and GO was partially reduced during the Fe
3
O
4
–GO preparation to produce Fe
3
O
4
–rGO. We propose plausible pathways for the Fe
3
O
4
formation, as well as a preliminary study on methylene blue degradation in water, using the Fe
3
O
4
–rGO nanocomposite.</description><identifier>ISSN: 0957-4522</identifier><identifier>EISSN: 1573-482X</identifier><identifier>DOI: 10.1007/s10854-020-02989-5</identifier><language>eng</language><publisher>New York: Springer US</publisher><subject>Characterization and Evaluation of Materials ; Chemistry and Materials Science ; Graphene ; Heavy metals ; Iron chlorides ; Iron oxides ; Magnetic properties ; Magnetite ; Materials Science ; Methylene blue ; Nanocomposites ; Nanoparticles ; Optical and Electronic Materials ; Structural analysis ; Ureas</subject><ispartof>Journal of materials science. Materials in electronics, 2020-05, Vol.31 (10), p.7490-7498</ispartof><rights>Springer Science+Business Media, LLC, part of Springer Nature 2020</rights><rights>Springer Science+Business Media, LLC, part of Springer Nature 2020.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c319t-f58809072f3a48fffa326785928c82fb66bc8ffbb4ede9752cd863fc0bd97cb23</citedby><cites>FETCH-LOGICAL-c319t-f58809072f3a48fffa326785928c82fb66bc8ffbb4ede9752cd863fc0bd97cb23</cites><orcidid>0000-0003-4208-150X</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>315,786,790,27957,27958</link.rule.ids></links><search><creatorcontrib>Pérez-Guzmán, M. A.</creatorcontrib><creatorcontrib>Ortega-Amaya, R.</creatorcontrib><creatorcontrib>Santoyo-Salazar, J.</creatorcontrib><creatorcontrib>Ortega-López, M.</creatorcontrib><title>Urea-based synthesis of magnetite nanoparticles and its composite with graphene oxide: structural and magnetic characterization</title><title>Journal of materials science. Materials in electronics</title><addtitle>J Mater Sci: Mater Electron</addtitle><description>Magnetite-loaded graphene oxide nanocomposites are currently studied as an easily retrievable efficient adsorbent of dyes and heavy metals. Therefore, the search for facile and low cost synthetical methods to prepare them is intensively pursued. This work describes a simple one-pot method to produce superparamagnetic magnetite nanoparticles (Fe
3
O
4
), and a hybrid nanocomposite of magnetite nanoparticles decorating reduced graphene oxide (Fe
3
O
4
–rGO) by reacting ferrous chloride with urea in water or graphene oxide–water dispersions, respectively. The synthetical method is based on temperature-assisted urea decomposition in water. The final products comprised Fe
3
O
4
nanoparticles or Fe
3
O
4
-decorated rGO sheets. Outstandingly, despite the polydisperse nature of Fe
3
O
4
, both materials are nearly superparamagnetic, and GO was partially reduced during the Fe
3
O
4
–GO preparation to produce Fe
3
O
4
–rGO. We propose plausible pathways for the Fe
3
O
4
formation, as well as a preliminary study on methylene blue degradation in water, using the Fe
3
O
4
–rGO nanocomposite.</description><subject>Characterization and Evaluation of Materials</subject><subject>Chemistry and Materials Science</subject><subject>Graphene</subject><subject>Heavy metals</subject><subject>Iron chlorides</subject><subject>Iron oxides</subject><subject>Magnetic properties</subject><subject>Magnetite</subject><subject>Materials Science</subject><subject>Methylene blue</subject><subject>Nanocomposites</subject><subject>Nanoparticles</subject><subject>Optical and Electronic Materials</subject><subject>Structural analysis</subject><subject>Ureas</subject><issn>0957-4522</issn><issn>1573-482X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2020</creationdate><recordtype>article</recordtype><recordid>eNp9kMtKxDAUhoMoOI6-gKuA62iaNG3iTgZvMODGAXchTZNphpmkJileNr66nQu4c3EInPzff-AD4LLA1wXG9U0qMGclwgSPI7hA7AhMClZTVHLydgwmWLAalYyQU3CW0gpjXJWUT8DPIhqFGpVMC9OXz51JLsFg4UYtvckuG-iVD72K2em1SVD5FrqcoA6bPqTt_4fLHVxG1XfGGxg-XWtuYcpx0HmIar0jDm0a6k5FpbOJ7ltlF_w5OLFqnczF4Z2CxcP96-wJzV8en2d3c6RpITKyjHMscE0sVSW31ipKqpozQbjmxDZV1ehx3TSlaY2oGdEtr6jVuGlFrRtCp-Bq39vH8D6YlOUqDNGPJyWhomI1L0Uxpsg-pWNIKRor--g2Kn7JAsutaLkXLUfRcidashGieyiNYb808a_6H-oXwCKEvA</recordid><startdate>20200501</startdate><enddate>20200501</enddate><creator>Pérez-Guzmán, M. 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A. ; Ortega-Amaya, R. ; Santoyo-Salazar, J. ; Ortega-López, M.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c319t-f58809072f3a48fffa326785928c82fb66bc8ffbb4ede9752cd863fc0bd97cb23</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2020</creationdate><topic>Characterization and Evaluation of Materials</topic><topic>Chemistry and Materials Science</topic><topic>Graphene</topic><topic>Heavy metals</topic><topic>Iron chlorides</topic><topic>Iron oxides</topic><topic>Magnetic properties</topic><topic>Magnetite</topic><topic>Materials Science</topic><topic>Methylene blue</topic><topic>Nanocomposites</topic><topic>Nanoparticles</topic><topic>Optical and Electronic Materials</topic><topic>Structural analysis</topic><topic>Ureas</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Pérez-Guzmán, M. A.</creatorcontrib><creatorcontrib>Ortega-Amaya, R.</creatorcontrib><creatorcontrib>Santoyo-Salazar, J.</creatorcontrib><creatorcontrib>Ortega-López, M.</creatorcontrib><collection>CrossRef</collection><collection>Electronics & Communications Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central</collection><collection>Advanced Technologies & Aerospace Database (1962 - current)</collection><collection>AUTh Library subscriptions: ProQuest Central</collection><collection>Technology Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central</collection><collection>ANTE: Abstracts in New Technology & Engineering</collection><collection>Engineering Research Database</collection><collection>SciTech Premium Collection (Proquest) (PQ_SDU_P3)</collection><collection>Materials Research Database</collection><collection>ProQuest Materials Science Database</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>ProQuest Advanced Technologies & Aerospace Database</collection><collection>ProQuest Advanced Technologies & Aerospace Collection</collection><collection>Materials Science Collection</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central China</collection><collection>DELNET Engineering & Technology Collection</collection><jtitle>Journal of materials science. Materials in electronics</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Pérez-Guzmán, M. A.</au><au>Ortega-Amaya, R.</au><au>Santoyo-Salazar, J.</au><au>Ortega-López, M.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Urea-based synthesis of magnetite nanoparticles and its composite with graphene oxide: structural and magnetic characterization</atitle><jtitle>Journal of materials science. Materials in electronics</jtitle><stitle>J Mater Sci: Mater Electron</stitle><date>2020-05-01</date><risdate>2020</risdate><volume>31</volume><issue>10</issue><spage>7490</spage><epage>7498</epage><pages>7490-7498</pages><issn>0957-4522</issn><eissn>1573-482X</eissn><abstract>Magnetite-loaded graphene oxide nanocomposites are currently studied as an easily retrievable efficient adsorbent of dyes and heavy metals. Therefore, the search for facile and low cost synthetical methods to prepare them is intensively pursued. This work describes a simple one-pot method to produce superparamagnetic magnetite nanoparticles (Fe
3
O
4
), and a hybrid nanocomposite of magnetite nanoparticles decorating reduced graphene oxide (Fe
3
O
4
–rGO) by reacting ferrous chloride with urea in water or graphene oxide–water dispersions, respectively. The synthetical method is based on temperature-assisted urea decomposition in water. The final products comprised Fe
3
O
4
nanoparticles or Fe
3
O
4
-decorated rGO sheets. Outstandingly, despite the polydisperse nature of Fe
3
O
4
, both materials are nearly superparamagnetic, and GO was partially reduced during the Fe
3
O
4
–GO preparation to produce Fe
3
O
4
–rGO. We propose plausible pathways for the Fe
3
O
4
formation, as well as a preliminary study on methylene blue degradation in water, using the Fe
3
O
4
–rGO nanocomposite.</abstract><cop>New York</cop><pub>Springer US</pub><doi>10.1007/s10854-020-02989-5</doi><tpages>9</tpages><orcidid>https://orcid.org/0000-0003-4208-150X</orcidid></addata></record> |
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| issn | 0957-4522 1573-482X |
| language | eng |
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| subjects | Characterization and Evaluation of Materials Chemistry and Materials Science Graphene Heavy metals Iron chlorides Iron oxides Magnetic properties Magnetite Materials Science Methylene blue Nanocomposites Nanoparticles Optical and Electronic Materials Structural analysis Ureas |
| title | Urea-based synthesis of magnetite nanoparticles and its composite with graphene oxide: structural and magnetic characterization |
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