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Fabrication of diamond whiskers by powder injection molding
Diamond whiskers with large aspect ratio and strong bonding strength were produced by powder injection molding. The main fabrication process were mixing, injection molding, debinding and sintering. Firstly, The diamond grits and Cu-Sn-Ti powders were mixed with a multi-components binder to prepare f...
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| Published in: | International journal of refractory metals & hard materials 2018-08, Vol.74, p.114-122 |
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| cited_by | cdi_FETCH-LOGICAL-c334t-c964d84260fd965007419a0e91c59242e303939df0662382f26aed9ab50f85823 |
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| cites | cdi_FETCH-LOGICAL-c334t-c964d84260fd965007419a0e91c59242e303939df0662382f26aed9ab50f85823 |
| container_end_page | 122 |
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| container_start_page | 114 |
| container_title | International journal of refractory metals & hard materials |
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| creator | Wu, Qiaoping Luo, Zhou Deng, Zhaohui Wang, Yu Fu, Zhiqiang |
| description | Diamond whiskers with large aspect ratio and strong bonding strength were produced by powder injection molding. The main fabrication process were mixing, injection molding, debinding and sintering. Firstly, The diamond grits and Cu-Sn-Ti powders were mixed with a multi-components binder to prepare feedstock. The feedstock was then injected into the mold cavity to form the green part with desired shape, and defect-free green parts were obtained by optimizing the injection molding parameters (injection pressure 12 MPa, injection temperature 165 °C and mold temperature 40 °C). Next, a solvent-thermal debinding process was employed to extract the binders in the green parts. Finally, The debound samples were sintered in vacuum atmosphere at 920 °C for 10 min to obtain diamond whiskers.The single whisker grinding test was carried out to discuss the cutting performance of diamond whiskers machining WC/12Co coating. The results indicated that diamond whisker had good cutting performance, and diamond grits in the diamond whisker mainly occurred integrity, micro-fracture, fracture and rubdown, diamond grits pullouts were not easy to happen due to the presence of the chemical bonding between the diamond grits and Cu-Sn-Ti alloy. And it has great potential to further prepare the diamond whiskers wheels which the diamond whiskers serving as the abrasives oriented radially in the wheel.
•Diamond whiskers with large aspect ratio and strong bonding strength were produced by powder injection molding.The main fabrication process were mixing, injection molding, debinding and sintering.•The diamonds and Cu-Sn-Ti powders were mixed with a multi-components binder to prepare feedstock. The feedstock was injected into the mold cavity to form the green part, and defect-free green parts were obtained by optimizing the injection molding parameters. Next, a solvent-thermal debinding was employed to extract the binders. Finally, The debound samples were sintered to obtain diamond whiskers.•The single whisker grinding test was carried out to discuss the cutting performance of diamond whiskers machining WC/12Co coating. The results indicated that diamond whisker had good cutting performance, and diamond grits were not easy to happen due to the presence of the chemical bonding between the diamond grits and Cu-Sn-Ti alloy.•Due to the large aspect ratio and strong bonding strength of the diamond whiskers, it has great potential to further prepare the diamond whiskers wheels which the diamo |
| doi_str_mv | 10.1016/j.ijrmhm.2018.03.009 |
| format | article |
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•Diamond whiskers with large aspect ratio and strong bonding strength were produced by powder injection molding.The main fabrication process were mixing, injection molding, debinding and sintering.•The diamonds and Cu-Sn-Ti powders were mixed with a multi-components binder to prepare feedstock. The feedstock was injected into the mold cavity to form the green part, and defect-free green parts were obtained by optimizing the injection molding parameters. Next, a solvent-thermal debinding was employed to extract the binders. Finally, The debound samples were sintered to obtain diamond whiskers.•The single whisker grinding test was carried out to discuss the cutting performance of diamond whiskers machining WC/12Co coating. The results indicated that diamond whisker had good cutting performance, and diamond grits were not easy to happen due to the presence of the chemical bonding between the diamond grits and Cu-Sn-Ti alloy.•Due to the large aspect ratio and strong bonding strength of the diamond whiskers, it has great potential to further prepare the diamond whiskers wheels which the diamond whiskers serving as the abrasives oriented radially in the wheel.</description><identifier>ISSN: 0263-4368</identifier><identifier>EISSN: 2213-3917</identifier><identifier>DOI: 10.1016/j.ijrmhm.2018.03.009</identifier><language>eng</language><publisher>Shrewsbury: Elsevier Ltd</publisher><subject>Abrasive wheels ; Abrasives ; Additive manufacturing ; Adhesives ; Aspect ratio ; Binder removal ; Bonding strength ; Chemical bonds ; Copper base alloys ; Cu-Sn-Ti powder ; Cutting ; Cutting forces ; Cutting performance ; Diamond machining ; Diamond whisker ; Injection molding ; Molding parameters ; Organic chemistry ; Powder injection molding ; Raw materials ; Sintering (powder metallurgy) ; Tungsten carbide ; Whiskers (metals)</subject><ispartof>International journal of refractory metals & hard materials, 2018-08, Vol.74, p.114-122</ispartof><rights>2018 Elsevier Ltd</rights><rights>Copyright Elsevier BV Aug 2018</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c334t-c964d84260fd965007419a0e91c59242e303939df0662382f26aed9ab50f85823</citedby><cites>FETCH-LOGICAL-c334t-c964d84260fd965007419a0e91c59242e303939df0662382f26aed9ab50f85823</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>315,786,790,27957,27958</link.rule.ids></links><search><creatorcontrib>Wu, Qiaoping</creatorcontrib><creatorcontrib>Luo, Zhou</creatorcontrib><creatorcontrib>Deng, Zhaohui</creatorcontrib><creatorcontrib>Wang, Yu</creatorcontrib><creatorcontrib>Fu, Zhiqiang</creatorcontrib><title>Fabrication of diamond whiskers by powder injection molding</title><title>International journal of refractory metals & hard materials</title><description>Diamond whiskers with large aspect ratio and strong bonding strength were produced by powder injection molding. The main fabrication process were mixing, injection molding, debinding and sintering. Firstly, The diamond grits and Cu-Sn-Ti powders were mixed with a multi-components binder to prepare feedstock. The feedstock was then injected into the mold cavity to form the green part with desired shape, and defect-free green parts were obtained by optimizing the injection molding parameters (injection pressure 12 MPa, injection temperature 165 °C and mold temperature 40 °C). Next, a solvent-thermal debinding process was employed to extract the binders in the green parts. Finally, The debound samples were sintered in vacuum atmosphere at 920 °C for 10 min to obtain diamond whiskers.The single whisker grinding test was carried out to discuss the cutting performance of diamond whiskers machining WC/12Co coating. The results indicated that diamond whisker had good cutting performance, and diamond grits in the diamond whisker mainly occurred integrity, micro-fracture, fracture and rubdown, diamond grits pullouts were not easy to happen due to the presence of the chemical bonding between the diamond grits and Cu-Sn-Ti alloy. And it has great potential to further prepare the diamond whiskers wheels which the diamond whiskers serving as the abrasives oriented radially in the wheel.
•Diamond whiskers with large aspect ratio and strong bonding strength were produced by powder injection molding.The main fabrication process were mixing, injection molding, debinding and sintering.•The diamonds and Cu-Sn-Ti powders were mixed with a multi-components binder to prepare feedstock. The feedstock was injected into the mold cavity to form the green part, and defect-free green parts were obtained by optimizing the injection molding parameters. Next, a solvent-thermal debinding was employed to extract the binders. Finally, The debound samples were sintered to obtain diamond whiskers.•The single whisker grinding test was carried out to discuss the cutting performance of diamond whiskers machining WC/12Co coating. The results indicated that diamond whisker had good cutting performance, and diamond grits were not easy to happen due to the presence of the chemical bonding between the diamond grits and Cu-Sn-Ti alloy.•Due to the large aspect ratio and strong bonding strength of the diamond whiskers, it has great potential to further prepare the diamond whiskers wheels which the diamond whiskers serving as the abrasives oriented radially in the wheel.</description><subject>Abrasive wheels</subject><subject>Abrasives</subject><subject>Additive manufacturing</subject><subject>Adhesives</subject><subject>Aspect ratio</subject><subject>Binder removal</subject><subject>Bonding strength</subject><subject>Chemical bonds</subject><subject>Copper base alloys</subject><subject>Cu-Sn-Ti powder</subject><subject>Cutting</subject><subject>Cutting forces</subject><subject>Cutting performance</subject><subject>Diamond machining</subject><subject>Diamond whisker</subject><subject>Injection molding</subject><subject>Molding parameters</subject><subject>Organic chemistry</subject><subject>Powder injection molding</subject><subject>Raw materials</subject><subject>Sintering (powder metallurgy)</subject><subject>Tungsten carbide</subject><subject>Whiskers (metals)</subject><issn>0263-4368</issn><issn>2213-3917</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2018</creationdate><recordtype>article</recordtype><recordid>eNp9kFFLwzAUhYMoOKf_wIeCz603uWnWIAgynAoDX_Q5ZEnqUtdmJp1j_97O-uzTffnOuZyPkGsKBQUqbpvCN7FdtwUDWhWABYA8IRPGKOYo6eyUTIAJzDmK6pxcpNQAgJCCTsjdQq-iN7r3octCnVmv29DZbL_26dPFlK0O2TbsrYuZ7xpnfrk2bKzvPi7JWa03yV393Sl5Xzy-zZ_z5evTy_xhmRtE3udGCm4rzgTUVooSYMap1OAkNaVknDkElChtDUIwrFjNhHZW6lUJdVVWDKfkZuzdxvC1c6lXTdjFbnipGEikElh5pPhImRhSiq5W2-hbHQ-KgjpqUo0aNamjJgWoBk1D7H6MuWHBt3dRJeNdZ5z1cZirbPD_F_wAIZBw5w</recordid><startdate>201808</startdate><enddate>201808</enddate><creator>Wu, Qiaoping</creator><creator>Luo, Zhou</creator><creator>Deng, Zhaohui</creator><creator>Wang, Yu</creator><creator>Fu, Zhiqiang</creator><general>Elsevier Ltd</general><general>Elsevier BV</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7QQ</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>201808</creationdate><title>Fabrication of diamond whiskers by powder injection molding</title><author>Wu, Qiaoping ; Luo, Zhou ; Deng, Zhaohui ; Wang, Yu ; Fu, Zhiqiang</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c334t-c964d84260fd965007419a0e91c59242e303939df0662382f26aed9ab50f85823</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2018</creationdate><topic>Abrasive wheels</topic><topic>Abrasives</topic><topic>Additive manufacturing</topic><topic>Adhesives</topic><topic>Aspect ratio</topic><topic>Binder removal</topic><topic>Bonding strength</topic><topic>Chemical bonds</topic><topic>Copper base alloys</topic><topic>Cu-Sn-Ti powder</topic><topic>Cutting</topic><topic>Cutting forces</topic><topic>Cutting performance</topic><topic>Diamond machining</topic><topic>Diamond whisker</topic><topic>Injection molding</topic><topic>Molding parameters</topic><topic>Organic chemistry</topic><topic>Powder injection molding</topic><topic>Raw materials</topic><topic>Sintering (powder metallurgy)</topic><topic>Tungsten carbide</topic><topic>Whiskers (metals)</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Wu, Qiaoping</creatorcontrib><creatorcontrib>Luo, Zhou</creatorcontrib><creatorcontrib>Deng, Zhaohui</creatorcontrib><creatorcontrib>Wang, Yu</creatorcontrib><creatorcontrib>Fu, Zhiqiang</creatorcontrib><collection>CrossRef</collection><collection>Ceramic Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>International journal of refractory metals & hard materials</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Wu, Qiaoping</au><au>Luo, Zhou</au><au>Deng, Zhaohui</au><au>Wang, Yu</au><au>Fu, Zhiqiang</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Fabrication of diamond whiskers by powder injection molding</atitle><jtitle>International journal of refractory metals & hard materials</jtitle><date>2018-08</date><risdate>2018</risdate><volume>74</volume><spage>114</spage><epage>122</epage><pages>114-122</pages><issn>0263-4368</issn><eissn>2213-3917</eissn><abstract>Diamond whiskers with large aspect ratio and strong bonding strength were produced by powder injection molding. The main fabrication process were mixing, injection molding, debinding and sintering. Firstly, The diamond grits and Cu-Sn-Ti powders were mixed with a multi-components binder to prepare feedstock. The feedstock was then injected into the mold cavity to form the green part with desired shape, and defect-free green parts were obtained by optimizing the injection molding parameters (injection pressure 12 MPa, injection temperature 165 °C and mold temperature 40 °C). Next, a solvent-thermal debinding process was employed to extract the binders in the green parts. Finally, The debound samples were sintered in vacuum atmosphere at 920 °C for 10 min to obtain diamond whiskers.The single whisker grinding test was carried out to discuss the cutting performance of diamond whiskers machining WC/12Co coating. The results indicated that diamond whisker had good cutting performance, and diamond grits in the diamond whisker mainly occurred integrity, micro-fracture, fracture and rubdown, diamond grits pullouts were not easy to happen due to the presence of the chemical bonding between the diamond grits and Cu-Sn-Ti alloy. And it has great potential to further prepare the diamond whiskers wheels which the diamond whiskers serving as the abrasives oriented radially in the wheel.
•Diamond whiskers with large aspect ratio and strong bonding strength were produced by powder injection molding.The main fabrication process were mixing, injection molding, debinding and sintering.•The diamonds and Cu-Sn-Ti powders were mixed with a multi-components binder to prepare feedstock. The feedstock was injected into the mold cavity to form the green part, and defect-free green parts were obtained by optimizing the injection molding parameters. Next, a solvent-thermal debinding was employed to extract the binders. Finally, The debound samples were sintered to obtain diamond whiskers.•The single whisker grinding test was carried out to discuss the cutting performance of diamond whiskers machining WC/12Co coating. The results indicated that diamond whisker had good cutting performance, and diamond grits were not easy to happen due to the presence of the chemical bonding between the diamond grits and Cu-Sn-Ti alloy.•Due to the large aspect ratio and strong bonding strength of the diamond whiskers, it has great potential to further prepare the diamond whiskers wheels which the diamond whiskers serving as the abrasives oriented radially in the wheel.</abstract><cop>Shrewsbury</cop><pub>Elsevier Ltd</pub><doi>10.1016/j.ijrmhm.2018.03.009</doi><tpages>9</tpages></addata></record> |
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| ispartof | International journal of refractory metals & hard materials, 2018-08, Vol.74, p.114-122 |
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| source | ScienceDirect Freedom Collection |
| subjects | Abrasive wheels Abrasives Additive manufacturing Adhesives Aspect ratio Binder removal Bonding strength Chemical bonds Copper base alloys Cu-Sn-Ti powder Cutting Cutting forces Cutting performance Diamond machining Diamond whisker Injection molding Molding parameters Organic chemistry Powder injection molding Raw materials Sintering (powder metallurgy) Tungsten carbide Whiskers (metals) |
| title | Fabrication of diamond whiskers by powder injection molding |
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