The Potential of Solid-State Nuclear Magnetic Resonance in Dairy Research: An Application to Cheese

Nuclear magnetic resonance spectroscopy is a noninvasive technique that has found application in a variety of research areas. Nuclear magnetic resonance has been primarily applied to solution studies, but many dairy food ingredients or products are solids. In this paper, cross-polarization magic ang...

Full description

Saved in:
Bibliographic Details
Published in:Journal of dairy science 1994-03, Vol.77 (3), p.667-671
Main Authors: Kakalis, L.T., Kumosinski, T.F., Farrell, H.M.
Format: Article
Language:English
Subjects:
Biological and medical sciences
cheese
espectroscopia rmn
Food industries
freeze drying
fromage
Fundamental and applied biological sciences. Psychology
liofilizacion
lyophilisation
Milk and cheese industries. Ice creams
nmr spectroscopy
nuclear magnetic resonance
queso
spectroscopie rmn
Citations: Items that this one cites
Items that cite this one
Online Access:Get full text
Tags: Add Tag
No Tags, Be the first to tag this record!
cited_by cdi_FETCH-LOGICAL-c482t-cddfc1c79fb6101ff49781d5ed3c8c355e70c54f5394364f182ff29ececeee223
cites cdi_FETCH-LOGICAL-c482t-cddfc1c79fb6101ff49781d5ed3c8c355e70c54f5394364f182ff29ececeee223
container_end_page 671
container_issue 3
container_start_page 667
container_title Journal of dairy science
container_volume 77
creator Kakalis, L.T.
Kumosinski, T.F.
Farrell, H.M.
description Nuclear magnetic resonance spectroscopy is a noninvasive technique that has found application in a variety of research areas. Nuclear magnetic resonance has been primarily applied to solution studies, but many dairy food ingredients or products are solids. In this paper, cross-polarization magic angle spinning nuclear magnetic resonance is applied to the study of freeze-dried cheese. The 13C spectrum is dominated by the solid-like protein fraction. Liquid-like fat resonances can be detected by conventional one pulse experiments. The 31P cross-polarization magic angle spinning nuclear magnetic resonance can specifically monitor phosphorus-containing ingredients in the solid state. Possible applications of solid-state nuclear magnetic resonance to dairy research are discussed.
doi_str_mv 10.3168/jds.S0022-0302(94)76997-6
format article
fullrecord <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_journals_1877151371</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><els_id>S0022030294769976</els_id><sourcerecordid>1877151371</sourcerecordid><originalsourceid>FETCH-LOGICAL-c482t-cddfc1c79fb6101ff49781d5ed3c8c355e70c54f5394364f182ff29ececeee223</originalsourceid><addsrcrecordid>eNqNkE1v1DAQhiMEEkvhLyAjQIJDiseO45jbavmUyofY9my5znjXqzQOthfUf4-zqXpGPow88_gd66mqF0DPObTdu0OfzreUMlZTTtkb1byVrVKybh9UKxBM1BxU97Ba3SOPqycpHcoVGBWryl7ukfwMGcfszUCCI9sw-L7eZpORfD_aAU0k38xuxOwt-YUpjGa0SPxIPhgfb-dWQez-PVmPZD1Ng7cm-zCSHMhmj2X6tHrkzJDw2V09q64-fbzcfKkvfnz-ullf1LbpWK5t3zsLVip33QIF5xolO-gF9tx2lguBklrROMFVw9vGQcecYwptOYiM8bPq5ZI7xfD7iCnrQzjGsazU0EkJAriEQqmFsjGkFNHpKfobE281UD071cWpPjnVszCtGn1yqtvy9tXdBpOsGVwsKny6D2hAtZTJgr1esL3f7f_6iDrdmGGYjtcwh0upuW7bmXu-cM4EbXaxRF1tQSlBgTX0BGwWAIu2Px6jTtZj0d-XUJt1H_x__PofQCejzg</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>1877151371</pqid></control><display><type>article</type><title>The Potential of Solid-State Nuclear Magnetic Resonance in Dairy Research: An Application to Cheese</title><source>EZB-FREE-00999 freely available EZB journals</source><creator>Kakalis, L.T. ; Kumosinski, T.F. ; Farrell, H.M.</creator><creatorcontrib>Kakalis, L.T. ; Kumosinski, T.F. ; Farrell, H.M.</creatorcontrib><description>Nuclear magnetic resonance spectroscopy is a noninvasive technique that has found application in a variety of research areas. Nuclear magnetic resonance has been primarily applied to solution studies, but many dairy food ingredients or products are solids. In this paper, cross-polarization magic angle spinning nuclear magnetic resonance is applied to the study of freeze-dried cheese. The 13C spectrum is dominated by the solid-like protein fraction. Liquid-like fat resonances can be detected by conventional one pulse experiments. The 31P cross-polarization magic angle spinning nuclear magnetic resonance can specifically monitor phosphorus-containing ingredients in the solid state. Possible applications of solid-state nuclear magnetic resonance to dairy research are discussed.</description><identifier>ISSN: 0022-0302</identifier><identifier>EISSN: 1525-3198</identifier><identifier>DOI: 10.3168/jds.S0022-0302(94)76997-6</identifier><identifier>CODEN: JDSCAE</identifier><language>eng</language><publisher>Savoy, IL: Elsevier Inc</publisher><subject>Biological and medical sciences ; cheese ; espectroscopia rmn ; Food industries ; freeze drying ; fromage ; Fundamental and applied biological sciences. Psychology ; liofilizacion ; lyophilisation ; Milk and cheese industries. Ice creams ; nmr spectroscopy ; nuclear magnetic resonance ; queso ; spectroscopie rmn</subject><ispartof>Journal of dairy science, 1994-03, Vol.77 (3), p.667-671</ispartof><rights>1994 American Dairy Science Association</rights><rights>1994 INIST-CNRS</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c482t-cddfc1c79fb6101ff49781d5ed3c8c355e70c54f5394364f182ff29ececeee223</citedby><cites>FETCH-LOGICAL-c482t-cddfc1c79fb6101ff49781d5ed3c8c355e70c54f5394364f182ff29ececeee223</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>315,786,790,27957,27958</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&amp;idt=4196027$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Kakalis, L.T.</creatorcontrib><creatorcontrib>Kumosinski, T.F.</creatorcontrib><creatorcontrib>Farrell, H.M.</creatorcontrib><title>The Potential of Solid-State Nuclear Magnetic Resonance in Dairy Research: An Application to Cheese</title><title>Journal of dairy science</title><description>Nuclear magnetic resonance spectroscopy is a noninvasive technique that has found application in a variety of research areas. Nuclear magnetic resonance has been primarily applied to solution studies, but many dairy food ingredients or products are solids. In this paper, cross-polarization magic angle spinning nuclear magnetic resonance is applied to the study of freeze-dried cheese. The 13C spectrum is dominated by the solid-like protein fraction. Liquid-like fat resonances can be detected by conventional one pulse experiments. The 31P cross-polarization magic angle spinning nuclear magnetic resonance can specifically monitor phosphorus-containing ingredients in the solid state. Possible applications of solid-state nuclear magnetic resonance to dairy research are discussed.</description><subject>Biological and medical sciences</subject><subject>cheese</subject><subject>espectroscopia rmn</subject><subject>Food industries</subject><subject>freeze drying</subject><subject>fromage</subject><subject>Fundamental and applied biological sciences. Psychology</subject><subject>liofilizacion</subject><subject>lyophilisation</subject><subject>Milk and cheese industries. Ice creams</subject><subject>nmr spectroscopy</subject><subject>nuclear magnetic resonance</subject><subject>queso</subject><subject>spectroscopie rmn</subject><issn>0022-0302</issn><issn>1525-3198</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>1994</creationdate><recordtype>article</recordtype><recordid>eNqNkE1v1DAQhiMEEkvhLyAjQIJDiseO45jbavmUyofY9my5znjXqzQOthfUf4-zqXpGPow88_gd66mqF0DPObTdu0OfzreUMlZTTtkb1byVrVKybh9UKxBM1BxU97Ba3SOPqycpHcoVGBWryl7ukfwMGcfszUCCI9sw-L7eZpORfD_aAU0k38xuxOwt-YUpjGa0SPxIPhgfb-dWQez-PVmPZD1Ng7cm-zCSHMhmj2X6tHrkzJDw2V09q64-fbzcfKkvfnz-ullf1LbpWK5t3zsLVip33QIF5xolO-gF9tx2lguBklrROMFVw9vGQcecYwptOYiM8bPq5ZI7xfD7iCnrQzjGsazU0EkJAriEQqmFsjGkFNHpKfobE281UD071cWpPjnVszCtGn1yqtvy9tXdBpOsGVwsKny6D2hAtZTJgr1esL3f7f_6iDrdmGGYjtcwh0upuW7bmXu-cM4EbXaxRF1tQSlBgTX0BGwWAIu2Px6jTtZj0d-XUJt1H_x__PofQCejzg</recordid><startdate>19940301</startdate><enddate>19940301</enddate><creator>Kakalis, L.T.</creator><creator>Kumosinski, T.F.</creator><creator>Farrell, H.M.</creator><general>Elsevier Inc</general><general>Am Dairy Sci Assoc</general><general>American Dairy Science Association</general><scope>6I.</scope><scope>AAFTH</scope><scope>FBQ</scope><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7WH</scope><scope>K30</scope><scope>PAAUG</scope><scope>PAWHS</scope><scope>PAWZZ</scope><scope>PAXOH</scope><scope>PBHAV</scope><scope>PBQSW</scope><scope>PBYQZ</scope><scope>PCIWU</scope><scope>PCMID</scope><scope>PCZJX</scope><scope>PDGRG</scope><scope>PDWWI</scope><scope>PETMR</scope><scope>PFVGT</scope><scope>PGXDX</scope><scope>PIHIL</scope><scope>PISVA</scope><scope>PJCTQ</scope><scope>PJTMS</scope><scope>PLCHJ</scope><scope>PMHAD</scope><scope>PNQDJ</scope><scope>POUND</scope><scope>PPLAD</scope><scope>PQAPC</scope><scope>PQCAN</scope><scope>PQCMW</scope><scope>PQEME</scope><scope>PQHKH</scope><scope>PQMID</scope><scope>PQNCT</scope><scope>PQNET</scope><scope>PQSCT</scope><scope>PQSET</scope><scope>PSVJG</scope><scope>PVMQY</scope><scope>PZGFC</scope></search><sort><creationdate>19940301</creationdate><title>The Potential of Solid-State Nuclear Magnetic Resonance in Dairy Research: An Application to Cheese</title><author>Kakalis, L.T. ; Kumosinski, T.F. ; Farrell, H.M.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c482t-cddfc1c79fb6101ff49781d5ed3c8c355e70c54f5394364f182ff29ececeee223</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>1994</creationdate><topic>Biological and medical sciences</topic><topic>cheese</topic><topic>espectroscopia rmn</topic><topic>Food industries</topic><topic>freeze drying</topic><topic>fromage</topic><topic>Fundamental and applied biological sciences. Psychology</topic><topic>liofilizacion</topic><topic>lyophilisation</topic><topic>Milk and cheese industries. Ice creams</topic><topic>nmr spectroscopy</topic><topic>nuclear magnetic resonance</topic><topic>queso</topic><topic>spectroscopie rmn</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Kakalis, L.T.</creatorcontrib><creatorcontrib>Kumosinski, T.F.</creatorcontrib><creatorcontrib>Farrell, H.M.</creatorcontrib><collection>ScienceDirect Open Access Titles</collection><collection>Elsevier:ScienceDirect:Open Access</collection><collection>AGRIS</collection><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>Periodicals Index Online Segment 50</collection><collection>Periodicals Index Online</collection><collection>Primary Sources Access—Foundation Edition (Plan E) - West</collection><collection>Primary Sources Access (Plan D) - International</collection><collection>Primary Sources Access &amp; Build (Plan A) - MEA</collection><collection>Primary Sources Access—Foundation Edition (Plan E) - Midwest</collection><collection>Primary Sources Access—Foundation Edition (Plan E) - Northeast</collection><collection>Primary Sources Access (Plan D) - Southeast</collection><collection>Primary Sources Access (Plan D) - North Central</collection><collection>Primary Sources Access—Foundation Edition (Plan E) - Southeast</collection><collection>Primary Sources Access (Plan D) - South Central</collection><collection>Primary Sources Access &amp; Build (Plan A) - UK / I</collection><collection>Primary Sources Access (Plan D) - Canada</collection><collection>Primary Sources Access (Plan D) - EMEALA</collection><collection>Primary Sources Access—Foundation Edition (Plan E) - North Central</collection><collection>Primary Sources Access—Foundation Edition (Plan E) - South Central</collection><collection>Primary Sources Access &amp; Build (Plan A) - International</collection><collection>Primary Sources Access—Foundation Edition (Plan E) - International</collection><collection>Primary Sources Access (Plan D) - West</collection><collection>Periodicals Index Online Segments 1-50</collection><collection>Primary Sources Access (Plan D) - APAC</collection><collection>Primary Sources Access (Plan D) - Midwest</collection><collection>Primary Sources Access (Plan D) - MEA</collection><collection>Primary Sources Access—Foundation Edition (Plan E) - Canada</collection><collection>Primary Sources Access—Foundation Edition (Plan E) - UK / I</collection><collection>Primary Sources Access—Foundation Edition (Plan E) - EMEALA</collection><collection>Primary Sources Access &amp; Build (Plan A) - APAC</collection><collection>Primary Sources Access &amp; Build (Plan A) - Canada</collection><collection>Primary Sources Access &amp; Build (Plan A) - West</collection><collection>Primary Sources Access &amp; Build (Plan A) - EMEALA</collection><collection>Primary Sources Access (Plan D) - Northeast</collection><collection>Primary Sources Access &amp; Build (Plan A) - Midwest</collection><collection>Primary Sources Access &amp; Build (Plan A) - North Central</collection><collection>Primary Sources Access &amp; Build (Plan A) - Northeast</collection><collection>Primary Sources Access &amp; Build (Plan A) - South Central</collection><collection>Primary Sources Access &amp; Build (Plan A) - Southeast</collection><collection>Primary Sources Access (Plan D) - UK / I</collection><collection>Primary Sources Access—Foundation Edition (Plan E) - APAC</collection><collection>Primary Sources Access—Foundation Edition (Plan E) - MEA</collection><jtitle>Journal of dairy science</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Kakalis, L.T.</au><au>Kumosinski, T.F.</au><au>Farrell, H.M.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>The Potential of Solid-State Nuclear Magnetic Resonance in Dairy Research: An Application to Cheese</atitle><jtitle>Journal of dairy science</jtitle><date>1994-03-01</date><risdate>1994</risdate><volume>77</volume><issue>3</issue><spage>667</spage><epage>671</epage><pages>667-671</pages><issn>0022-0302</issn><eissn>1525-3198</eissn><coden>JDSCAE</coden><notes>Q</notes><notes>Q02</notes><abstract>Nuclear magnetic resonance spectroscopy is a noninvasive technique that has found application in a variety of research areas. Nuclear magnetic resonance has been primarily applied to solution studies, but many dairy food ingredients or products are solids. In this paper, cross-polarization magic angle spinning nuclear magnetic resonance is applied to the study of freeze-dried cheese. The 13C spectrum is dominated by the solid-like protein fraction. Liquid-like fat resonances can be detected by conventional one pulse experiments. The 31P cross-polarization magic angle spinning nuclear magnetic resonance can specifically monitor phosphorus-containing ingredients in the solid state. Possible applications of solid-state nuclear magnetic resonance to dairy research are discussed.</abstract><cop>Savoy, IL</cop><pub>Elsevier Inc</pub><doi>10.3168/jds.S0022-0302(94)76997-6</doi><tpages>5</tpages><oa>free_for_read</oa></addata></record>
fulltext fulltext
identifier ISSN: 0022-0302
ispartof Journal of dairy science, 1994-03, Vol.77 (3), p.667-671
issn 0022-0302
1525-3198
language eng
recordid cdi_proquest_journals_1877151371
source EZB-FREE-00999 freely available EZB journals
subjects Biological and medical sciences
cheese
espectroscopia rmn
Food industries
freeze drying
fromage
Fundamental and applied biological sciences. Psychology
liofilizacion
lyophilisation
Milk and cheese industries. Ice creams
nmr spectroscopy
nuclear magnetic resonance
queso
spectroscopie rmn
title The Potential of Solid-State Nuclear Magnetic Resonance in Dairy Research: An Application to Cheese
url http://sfxeu10.hosted.exlibrisgroup.com/loughborough?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2024-09-21T20%3A39%3A59IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=The%20Potential%20of%20Solid-State%20Nuclear%20Magnetic%20Resonance%20in%20Dairy%20Research:%20An%20Application%20to%20Cheese&rft.jtitle=Journal%20of%20dairy%20science&rft.au=Kakalis,%20L.T.&rft.date=1994-03-01&rft.volume=77&rft.issue=3&rft.spage=667&rft.epage=671&rft.pages=667-671&rft.issn=0022-0302&rft.eissn=1525-3198&rft.coden=JDSCAE&rft_id=info:doi/10.3168/jds.S0022-0302(94)76997-6&rft_dat=%3Cproquest_cross%3E1877151371%3C/proquest_cross%3E%3Cgrp_id%3Ecdi_FETCH-LOGICAL-c482t-cddfc1c79fb6101ff49781d5ed3c8c355e70c54f5394364f182ff29ececeee223%3C/grp_id%3E%3Coa%3E%3C/oa%3E%3Curl%3E%3C/url%3E&rft_id=info:oai/&rft_pqid=1877151371&rft_id=info:pmid/&rfr_iscdi=true