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Synthetic nanoclays with the structure of montmorillonite: Preparation, structure, and physico-chemical properties
Nanosized layered silicates with a montmorillonite structure of varying composition were synthesized under hydrothermal conditions (350°C, 700 atm). The hydrothermal treatment was applied to gels with the compositions calculated with the use of an ideal formula of the final product Na 2 x (Al 2(1 −...
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| Published in: | Glass physics and chemistry 2013-10, Vol.39 (5), p.533-539 |
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| Main Authors: | , , , , |
| Format: | Article |
| Language: | English |
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| cited_by | cdi_FETCH-LOGICAL-c316t-2be4a560e4874a6b87f01854beb6181af8e2960198d0a452d10de0d40dcd135b3 |
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| cites | cdi_FETCH-LOGICAL-c316t-2be4a560e4874a6b87f01854beb6181af8e2960198d0a452d10de0d40dcd135b3 |
| container_end_page | 539 |
| container_issue | 5 |
| container_start_page | 533 |
| container_title | Glass physics and chemistry |
| container_volume | 39 |
| creator | Golubeva, O. Yu Ul’yanova, N. Yu Kostyreva, T. G. Drozdova, I. A. Mokeev, M. V. |
| description | Nanosized layered silicates with a montmorillonite structure of varying composition were synthesized under hydrothermal conditions (350°C, 700 atm). The hydrothermal treatment was applied to gels with the compositions calculated with the use of an ideal formula of the final product Na
2
x
(Al
2(1 −
x
)
, Mg
2
x
) Si
4
O
10
(OH)
2
·
n
H
2
O (0 ≤
x
≤ 1). The obtained samples were investigated by X-ray diffraction, IR and NMR spectroscopy, electron microscopy, and mercury porosimetry. The values of the cation-exchange capacity and specific surface are determined. The mean size of the particles of the synthesized samples is 40 ± 7 nm. A gradual substitution of aluminum for part of the magnesium in the initial gel made it possible to obtain samples with well-defined composition-dependent characteristics. |
| doi_str_mv | 10.1134/S1087659613050088 |
| format | article |
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2
x
(Al
2(1 −
x
)
, Mg
2
x
) Si
4
O
10
(OH)
2
·
n
H
2
O (0 ≤
x
≤ 1). The obtained samples were investigated by X-ray diffraction, IR and NMR spectroscopy, electron microscopy, and mercury porosimetry. The values of the cation-exchange capacity and specific surface are determined. The mean size of the particles of the synthesized samples is 40 ± 7 nm. A gradual substitution of aluminum for part of the magnesium in the initial gel made it possible to obtain samples with well-defined composition-dependent characteristics.</description><identifier>ISSN: 1087-6596</identifier><identifier>EISSN: 1608-313X</identifier><identifier>DOI: 10.1134/S1087659613050088</identifier><language>eng</language><publisher>Boston: Springer US</publisher><subject>Ceramics ; Characterization and Evaluation of Materials ; Chemistry and Materials Science ; Composites ; Glass ; Materials Science ; Natural Materials ; Physical Chemistry</subject><ispartof>Glass physics and chemistry, 2013-10, Vol.39 (5), p.533-539</ispartof><rights>Pleiades Publishing, Ltd. 2013</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c316t-2be4a560e4874a6b87f01854beb6181af8e2960198d0a452d10de0d40dcd135b3</citedby><cites>FETCH-LOGICAL-c316t-2be4a560e4874a6b87f01854beb6181af8e2960198d0a452d10de0d40dcd135b3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>315,786,790,27957,27958</link.rule.ids></links><search><creatorcontrib>Golubeva, O. Yu</creatorcontrib><creatorcontrib>Ul’yanova, N. Yu</creatorcontrib><creatorcontrib>Kostyreva, T. G.</creatorcontrib><creatorcontrib>Drozdova, I. A.</creatorcontrib><creatorcontrib>Mokeev, M. V.</creatorcontrib><title>Synthetic nanoclays with the structure of montmorillonite: Preparation, structure, and physico-chemical properties</title><title>Glass physics and chemistry</title><addtitle>Glass Phys Chem</addtitle><description>Nanosized layered silicates with a montmorillonite structure of varying composition were synthesized under hydrothermal conditions (350°C, 700 atm). The hydrothermal treatment was applied to gels with the compositions calculated with the use of an ideal formula of the final product Na
2
x
(Al
2(1 −
x
)
, Mg
2
x
) Si
4
O
10
(OH)
2
·
n
H
2
O (0 ≤
x
≤ 1). The obtained samples were investigated by X-ray diffraction, IR and NMR spectroscopy, electron microscopy, and mercury porosimetry. The values of the cation-exchange capacity and specific surface are determined. The mean size of the particles of the synthesized samples is 40 ± 7 nm. A gradual substitution of aluminum for part of the magnesium in the initial gel made it possible to obtain samples with well-defined composition-dependent characteristics.</description><subject>Ceramics</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemistry and Materials Science</subject><subject>Composites</subject><subject>Glass</subject><subject>Materials Science</subject><subject>Natural Materials</subject><subject>Physical Chemistry</subject><issn>1087-6596</issn><issn>1608-313X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2013</creationdate><recordtype>article</recordtype><recordid>eNp1kE9LxDAQxYsouK5-AG8Br1udadM09SaL_2BBYRW8lTRNbZY2qUkW6be3ywoK4mmGeb_3HkwUnSNcIqb0ao3Ac5YVDFPIADg_iGbIgMcppm-H0z7J8U4_jk683wBAked0Frn1aEKrgpbECGNlJ0ZPPnVoyXQlPritDFuniG1Ib03ordNdZ40O6po8OzUIJ4K2ZvGDLogwNRna0WtpY9mqXkvRkcHZQbmglT-NjhrReXX2PefR693ty_IhXj3dPy5vVrFMkYU4qRQVGQNFeU4Fq3jeAPKMVqpiyFE0XCUFAyx4DYJmSY1QK6gp1LLGNKvSeXSxz52qP7bKh3Jjt85MlSVSimlBiySbKNxT0lnvnWrKweleuLFEKHevLf-8dvIke4-fWPOu3K_kf01fQpt9OA</recordid><startdate>20131001</startdate><enddate>20131001</enddate><creator>Golubeva, O. Yu</creator><creator>Ul’yanova, N. Yu</creator><creator>Kostyreva, T. G.</creator><creator>Drozdova, I. A.</creator><creator>Mokeev, M. V.</creator><general>Springer US</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7QQ</scope><scope>7SR</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>20131001</creationdate><title>Synthetic nanoclays with the structure of montmorillonite: Preparation, structure, and physico-chemical properties</title><author>Golubeva, O. Yu ; Ul’yanova, N. Yu ; Kostyreva, T. G. ; Drozdova, I. A. ; Mokeev, M. V.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c316t-2be4a560e4874a6b87f01854beb6181af8e2960198d0a452d10de0d40dcd135b3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2013</creationdate><topic>Ceramics</topic><topic>Characterization and Evaluation of Materials</topic><topic>Chemistry and Materials Science</topic><topic>Composites</topic><topic>Glass</topic><topic>Materials Science</topic><topic>Natural Materials</topic><topic>Physical Chemistry</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Golubeva, O. Yu</creatorcontrib><creatorcontrib>Ul’yanova, N. Yu</creatorcontrib><creatorcontrib>Kostyreva, T. G.</creatorcontrib><creatorcontrib>Drozdova, I. A.</creatorcontrib><creatorcontrib>Mokeev, M. V.</creatorcontrib><collection>CrossRef</collection><collection>Ceramic Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Glass physics and chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Golubeva, O. Yu</au><au>Ul’yanova, N. Yu</au><au>Kostyreva, T. G.</au><au>Drozdova, I. A.</au><au>Mokeev, M. V.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthetic nanoclays with the structure of montmorillonite: Preparation, structure, and physico-chemical properties</atitle><jtitle>Glass physics and chemistry</jtitle><stitle>Glass Phys Chem</stitle><date>2013-10-01</date><risdate>2013</risdate><volume>39</volume><issue>5</issue><spage>533</spage><epage>539</epage><pages>533-539</pages><issn>1087-6596</issn><eissn>1608-313X</eissn><abstract>Nanosized layered silicates with a montmorillonite structure of varying composition were synthesized under hydrothermal conditions (350°C, 700 atm). The hydrothermal treatment was applied to gels with the compositions calculated with the use of an ideal formula of the final product Na
2
x
(Al
2(1 −
x
)
, Mg
2
x
) Si
4
O
10
(OH)
2
·
n
H
2
O (0 ≤
x
≤ 1). The obtained samples were investigated by X-ray diffraction, IR and NMR spectroscopy, electron microscopy, and mercury porosimetry. The values of the cation-exchange capacity and specific surface are determined. The mean size of the particles of the synthesized samples is 40 ± 7 nm. A gradual substitution of aluminum for part of the magnesium in the initial gel made it possible to obtain samples with well-defined composition-dependent characteristics.</abstract><cop>Boston</cop><pub>Springer US</pub><doi>10.1134/S1087659613050088</doi><tpages>7</tpages></addata></record> |
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| ispartof | Glass physics and chemistry, 2013-10, Vol.39 (5), p.533-539 |
| issn | 1087-6596 1608-313X |
| language | eng |
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| source | Springer Link |
| subjects | Ceramics Characterization and Evaluation of Materials Chemistry and Materials Science Composites Glass Materials Science Natural Materials Physical Chemistry |
| title | Synthetic nanoclays with the structure of montmorillonite: Preparation, structure, and physico-chemical properties |
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