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Nanoscale characterization and formation mechanism of nanoclusters in an ODS steel elaborated by reactive-inspired ball-milling and annealing
Reactive-inspired ball-milling is proposed as a new production route for oxide dispersion strengthened (ODS) steels. So a Fe–14Cr–2W–1Ti–0.8Y–0.2O (wt.%) ODS steel is elaborated by ball-milling of FeCrWTi and YFe 3 plus Fe 2O 3 powders instead of Y 2O 3 and then by annealing at 800 °C for 5 min. Cha...
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| Published in: | Journal of nuclear materials 2011-02, Vol.409 (2), p.80-85 |
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| Main Authors: | , , , , , |
| Format: | Article |
| Language: | English |
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| cited_by | cdi_FETCH-LOGICAL-c504t-ba814c76fb533f15e0d5ced8bf911cfc7234d28863ad77dce617a5db35b759493 |
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| cites | cdi_FETCH-LOGICAL-c504t-ba814c76fb533f15e0d5ced8bf911cfc7234d28863ad77dce617a5db35b759493 |
| container_end_page | 85 |
| container_issue | 2 |
| container_start_page | 80 |
| container_title | Journal of nuclear materials |
| container_volume | 409 |
| creator | Brocq, M. Radiguet, B. Poissonnet, S. Cuvilly, F. Pareige, P. Legendre, F. |
| description | Reactive-inspired ball-milling is proposed as a new production route for oxide dispersion strengthened (ODS) steels. So a Fe–14Cr–2W–1Ti–0.8Y–0.2O
(wt.%) ODS steel is elaborated by ball-milling of FeCrWTi and YFe
3 plus Fe
2O
3 powders instead of Y
2O
3 and then by annealing at 800
°C for 5
min. Characterizations by Electron Probe MicroAnalysis and Atom Probe Tomography (APT) are performed after milling and after annealing. For the very first time, nanoclusters are observed after ball-milling by APT. Those nanoclusters are enriched in titanium, yttrium and oxygen and their mean radius is 0.8
nm. With annealing, the mean radius rises up to 1.4
nm and the number density as well as the enrichment factor in O, Ti and Y increase. So a new formation mechanism of nanoclusters is observed in those conditions of synthesis: ball-milling initiates the nanoclusters nucleation and during annealing, nucleation continues, accompanied by a slight growth of nanoclusters. Thus reactive-inspired ball-milling appears as a promising route for synthesizing ODS steels with a fine and dense dispersion of oxides. |
| doi_str_mv | 10.1016/j.jnucmat.2010.09.011 |
| format | article |
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(wt.%) ODS steel is elaborated by ball-milling of FeCrWTi and YFe
3 plus Fe
2O
3 powders instead of Y
2O
3 and then by annealing at 800
°C for 5
min. Characterizations by Electron Probe MicroAnalysis and Atom Probe Tomography (APT) are performed after milling and after annealing. For the very first time, nanoclusters are observed after ball-milling by APT. Those nanoclusters are enriched in titanium, yttrium and oxygen and their mean radius is 0.8
nm. With annealing, the mean radius rises up to 1.4
nm and the number density as well as the enrichment factor in O, Ti and Y increase. So a new formation mechanism of nanoclusters is observed in those conditions of synthesis: ball-milling initiates the nanoclusters nucleation and during annealing, nucleation continues, accompanied by a slight growth of nanoclusters. Thus reactive-inspired ball-milling appears as a promising route for synthesizing ODS steels with a fine and dense dispersion of oxides.</description><identifier>ISSN: 0022-3115</identifier><identifier>EISSN: 1873-4820</identifier><identifier>DOI: 10.1016/j.jnucmat.2010.09.011</identifier><identifier>CODEN: JNUMAM</identifier><language>eng</language><publisher>Amsterdam: Elsevier B.V</publisher><subject>Annealing ; Applied sciences ; Condensed Matter ; Controled nuclear fusion plants ; Dispersion hardening alloys ; Dispersions ; Energy ; Energy. Thermal use of fuels ; Exact sciences and technology ; Fission nuclear power plants ; Fuels ; Installations for energy generation and conversion: thermal and electrical energy ; Materials Science ; Milling (machining) ; Nanocomposites ; Nanomaterials ; Nanostructure ; Nuclear fuels ; Physics ; Steels</subject><ispartof>Journal of nuclear materials, 2011-02, Vol.409 (2), p.80-85</ispartof><rights>2010 Elsevier B.V.</rights><rights>2015 INIST-CNRS</rights><rights>Distributed under a Creative Commons Attribution 4.0 International License</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c504t-ba814c76fb533f15e0d5ced8bf911cfc7234d28863ad77dce617a5db35b759493</citedby><cites>FETCH-LOGICAL-c504t-ba814c76fb533f15e0d5ced8bf911cfc7234d28863ad77dce617a5db35b759493</cites><orcidid>0000-0002-5468-0887 ; 0000-0002-8722-8889</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>230,310,311,315,786,790,795,796,891,23958,23959,25170,27957,27958</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=23955285$$DView record in Pascal Francis$$Hfree_for_read</backlink><backlink>$$Uhttps://normandie-univ.hal.science/hal-02176567$$DView record in HAL$$Hfree_for_read</backlink></links><search><creatorcontrib>Brocq, M.</creatorcontrib><creatorcontrib>Radiguet, B.</creatorcontrib><creatorcontrib>Poissonnet, S.</creatorcontrib><creatorcontrib>Cuvilly, F.</creatorcontrib><creatorcontrib>Pareige, P.</creatorcontrib><creatorcontrib>Legendre, F.</creatorcontrib><title>Nanoscale characterization and formation mechanism of nanoclusters in an ODS steel elaborated by reactive-inspired ball-milling and annealing</title><title>Journal of nuclear materials</title><description>Reactive-inspired ball-milling is proposed as a new production route for oxide dispersion strengthened (ODS) steels. So a Fe–14Cr–2W–1Ti–0.8Y–0.2O
(wt.%) ODS steel is elaborated by ball-milling of FeCrWTi and YFe
3 plus Fe
2O
3 powders instead of Y
2O
3 and then by annealing at 800
°C for 5
min. Characterizations by Electron Probe MicroAnalysis and Atom Probe Tomography (APT) are performed after milling and after annealing. For the very first time, nanoclusters are observed after ball-milling by APT. Those nanoclusters are enriched in titanium, yttrium and oxygen and their mean radius is 0.8
nm. With annealing, the mean radius rises up to 1.4
nm and the number density as well as the enrichment factor in O, Ti and Y increase. So a new formation mechanism of nanoclusters is observed in those conditions of synthesis: ball-milling initiates the nanoclusters nucleation and during annealing, nucleation continues, accompanied by a slight growth of nanoclusters. Thus reactive-inspired ball-milling appears as a promising route for synthesizing ODS steels with a fine and dense dispersion of oxides.</description><subject>Annealing</subject><subject>Applied sciences</subject><subject>Condensed Matter</subject><subject>Controled nuclear fusion plants</subject><subject>Dispersion hardening alloys</subject><subject>Dispersions</subject><subject>Energy</subject><subject>Energy. Thermal use of fuels</subject><subject>Exact sciences and technology</subject><subject>Fission nuclear power plants</subject><subject>Fuels</subject><subject>Installations for energy generation and conversion: thermal and electrical energy</subject><subject>Materials Science</subject><subject>Milling (machining)</subject><subject>Nanocomposites</subject><subject>Nanomaterials</subject><subject>Nanostructure</subject><subject>Nuclear fuels</subject><subject>Physics</subject><subject>Steels</subject><issn>0022-3115</issn><issn>1873-4820</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2011</creationdate><recordtype>article</recordtype><recordid>eNqFkcFu1DAQhiMEEkvhEZB8QcAhy9iO4-SEqhYo0ooegLM1cSbUK8dZ7OxK5R14Zxyy6hFOo3_0zT-j-YviJYctB16_22_34WhHnLcCcg_aLXD-qNjwRsuyagQ8LjYAQpSSc_W0eJbSHgBUC2pT_P6CYUoWPTF7hxHtTNH9wtlNgWHo2TDFcVUjZSC4NLJpYCFPWX9MmU7MLSi7vf7KsibPyGM3RZypZ909i5RN3YlKF9LBxaWJ3pej896FH3-XYAiEi3pePBnQJ3pxrhfF948fvl3dlLvbT5-vLnelVVDNZYcNr6yuh05JOXBF0CtLfdMNLed2sFrIqhdNU0vste4t1Vyj6jupOq3aqpUXxdvV9w69OUQ3Yrw3Ezpzc7kzSw8E17Wq9Yln9vXKHuL080hpNqNLlrzHQNMxmabN7hqEzOSbf5LZUnABNSwHqBW1cUop0vBwBQezhGr25hyqWUI10Jocap57dV6BS2hDxGBdehgWslVKNCpz71eO8hdPjqJJ1lHIT8oJ2Nn0k_vPpj86Lrxs</recordid><startdate>20110215</startdate><enddate>20110215</enddate><creator>Brocq, M.</creator><creator>Radiguet, B.</creator><creator>Poissonnet, S.</creator><creator>Cuvilly, F.</creator><creator>Pareige, P.</creator><creator>Legendre, F.</creator><general>Elsevier B.V</general><general>Elsevier</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>7TB</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>FR3</scope><scope>JG9</scope><scope>L7M</scope><scope>7ST</scope><scope>C1K</scope><scope>SOI</scope><scope>1XC</scope><orcidid>https://orcid.org/0000-0002-5468-0887</orcidid><orcidid>https://orcid.org/0000-0002-8722-8889</orcidid></search><sort><creationdate>20110215</creationdate><title>Nanoscale characterization and formation mechanism of nanoclusters in an ODS steel elaborated by reactive-inspired ball-milling and annealing</title><author>Brocq, M. ; Radiguet, B. ; Poissonnet, S. ; Cuvilly, F. ; Pareige, P. ; Legendre, F.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c504t-ba814c76fb533f15e0d5ced8bf911cfc7234d28863ad77dce617a5db35b759493</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2011</creationdate><topic>Annealing</topic><topic>Applied sciences</topic><topic>Condensed Matter</topic><topic>Controled nuclear fusion plants</topic><topic>Dispersion hardening alloys</topic><topic>Dispersions</topic><topic>Energy</topic><topic>Energy. Thermal use of fuels</topic><topic>Exact sciences and technology</topic><topic>Fission nuclear power plants</topic><topic>Fuels</topic><topic>Installations for energy generation and conversion: thermal and electrical energy</topic><topic>Materials Science</topic><topic>Milling (machining)</topic><topic>Nanocomposites</topic><topic>Nanomaterials</topic><topic>Nanostructure</topic><topic>Nuclear fuels</topic><topic>Physics</topic><topic>Steels</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Brocq, M.</creatorcontrib><creatorcontrib>Radiguet, B.</creatorcontrib><creatorcontrib>Poissonnet, S.</creatorcontrib><creatorcontrib>Cuvilly, F.</creatorcontrib><creatorcontrib>Pareige, P.</creatorcontrib><creatorcontrib>Legendre, F.</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Mechanical & Transportation Engineering Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Engineering Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>Environment Abstracts</collection><collection>Environmental Sciences and Pollution Management</collection><collection>Environment Abstracts</collection><collection>Hyper Article en Ligne (HAL)</collection><jtitle>Journal of nuclear materials</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Brocq, M.</au><au>Radiguet, B.</au><au>Poissonnet, S.</au><au>Cuvilly, F.</au><au>Pareige, P.</au><au>Legendre, F.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Nanoscale characterization and formation mechanism of nanoclusters in an ODS steel elaborated by reactive-inspired ball-milling and annealing</atitle><jtitle>Journal of nuclear materials</jtitle><date>2011-02-15</date><risdate>2011</risdate><volume>409</volume><issue>2</issue><spage>80</spage><epage>85</epage><pages>80-85</pages><issn>0022-3115</issn><eissn>1873-4820</eissn><coden>JNUMAM</coden><notes>ObjectType-Article-1</notes><notes>SourceType-Scholarly Journals-1</notes><notes>ObjectType-Feature-2</notes><notes>content type line 23</notes><abstract>Reactive-inspired ball-milling is proposed as a new production route for oxide dispersion strengthened (ODS) steels. So a Fe–14Cr–2W–1Ti–0.8Y–0.2O
(wt.%) ODS steel is elaborated by ball-milling of FeCrWTi and YFe
3 plus Fe
2O
3 powders instead of Y
2O
3 and then by annealing at 800
°C for 5
min. Characterizations by Electron Probe MicroAnalysis and Atom Probe Tomography (APT) are performed after milling and after annealing. For the very first time, nanoclusters are observed after ball-milling by APT. Those nanoclusters are enriched in titanium, yttrium and oxygen and their mean radius is 0.8
nm. With annealing, the mean radius rises up to 1.4
nm and the number density as well as the enrichment factor in O, Ti and Y increase. So a new formation mechanism of nanoclusters is observed in those conditions of synthesis: ball-milling initiates the nanoclusters nucleation and during annealing, nucleation continues, accompanied by a slight growth of nanoclusters. Thus reactive-inspired ball-milling appears as a promising route for synthesizing ODS steels with a fine and dense dispersion of oxides.</abstract><cop>Amsterdam</cop><pub>Elsevier B.V</pub><doi>10.1016/j.jnucmat.2010.09.011</doi><tpages>6</tpages><orcidid>https://orcid.org/0000-0002-5468-0887</orcidid><orcidid>https://orcid.org/0000-0002-8722-8889</orcidid></addata></record> |
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| ispartof | Journal of nuclear materials, 2011-02, Vol.409 (2), p.80-85 |
| issn | 0022-3115 1873-4820 |
| language | eng |
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| source | ScienceDirect Journals |
| subjects | Annealing Applied sciences Condensed Matter Controled nuclear fusion plants Dispersion hardening alloys Dispersions Energy Energy. Thermal use of fuels Exact sciences and technology Fission nuclear power plants Fuels Installations for energy generation and conversion: thermal and electrical energy Materials Science Milling (machining) Nanocomposites Nanomaterials Nanostructure Nuclear fuels Physics Steels |
| title | Nanoscale characterization and formation mechanism of nanoclusters in an ODS steel elaborated by reactive-inspired ball-milling and annealing |
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