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High resolution Transmission Electron Microscopy characterization of a milled oxide dispersion strengthened steel powder
Oxide Dispersion Strengthened (ODS) steels are promising materials for generation IV fuel claddings as their dense nano-oxide dispersion provides good creep and irradiation resistance. Even if they have been studied for years, the formation mechanism of these nano-oxides is still unclear. Here we re...
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Published in: | Journal of nuclear materials 2016-10, Vol.479, p.76-84 |
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container_title | Journal of nuclear materials |
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creator | Loyer-Prost, M. Merot, J.-S. Ribis, J. Le Bouar, Y. Chaffron, L. Legendre, F. |
description | Oxide Dispersion Strengthened (ODS) steels are promising materials for generation IV fuel claddings as their dense nano-oxide dispersion provides good creep and irradiation resistance. Even if they have been studied for years, the formation mechanism of these nano-oxides is still unclear. Here we report for the first time a High Resolution Transmission Electron Microscopy and Energy Filtered Transmission Electron Microscopy characterization of an ODS milled powder. It provides clear evidence of the presence of small crystalline nanoclusters (NCs) enriched in titanium directly after milling. Small NCs ( |
doi_str_mv | 10.1016/j.jnucmat.2016.06.050 |
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•We observed an ODS ball-milled powder by high resolution transmission microscopy.•The ODS ball-milled powder exhibits a lamellar microstructure.•Small crystalline nanoclusters were detected in the milled ODS powder.•The nanoclusters in the ODS milled powder are enriched in titanium.•Larger NCs of 15–20 nm in size are, at least, partly coherent with the matrix.</description><identifier>ISSN: 0022-3115</identifier><identifier>EISSN: 1873-4820</identifier><identifier>DOI: 10.1016/j.jnucmat.2016.06.050</identifier><language>eng</language><publisher>Elsevier B.V</publisher><subject>Ball-milling ; Engineering Sciences ; Materials ; Nanostructured materials ; ODS ferritic steel ; Powder characterization ; Transmission Electron Microscopy</subject><ispartof>Journal of nuclear materials, 2016-10, Vol.479, p.76-84</ispartof><rights>2016 Elsevier B.V.</rights><rights>Distributed under a Creative Commons Attribution 4.0 International License</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c409t-467b0c078fd5d9bd9549819b17d563a68ca915645ffecaa4d2a32059030738983</citedby><cites>FETCH-LOGICAL-c409t-467b0c078fd5d9bd9549819b17d563a68ca915645ffecaa4d2a32059030738983</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>230,315,786,790,891,27957,27958</link.rule.ids><backlink>$$Uhttps://hal.science/hal-01403043$$DView record in HAL$$Hfree_for_read</backlink></links><search><creatorcontrib>Loyer-Prost, M.</creatorcontrib><creatorcontrib>Merot, J.-S.</creatorcontrib><creatorcontrib>Ribis, J.</creatorcontrib><creatorcontrib>Le Bouar, Y.</creatorcontrib><creatorcontrib>Chaffron, L.</creatorcontrib><creatorcontrib>Legendre, F.</creatorcontrib><title>High resolution Transmission Electron Microscopy characterization of a milled oxide dispersion strengthened steel powder</title><title>Journal of nuclear materials</title><description>Oxide Dispersion Strengthened (ODS) steels are promising materials for generation IV fuel claddings as their dense nano-oxide dispersion provides good creep and irradiation resistance. Even if they have been studied for years, the formation mechanism of these nano-oxides is still unclear. Here we report for the first time a High Resolution Transmission Electron Microscopy and Energy Filtered Transmission Electron Microscopy characterization of an ODS milled powder. It provides clear evidence of the presence of small crystalline nanoclusters (NCs) enriched in titanium directly after milling. Small NCs (<5 nm) have a crystalline structure and seem partly coherent with the matrix. They have an interplanar spacing close to the (011) bcc iron structure. They coexist with larger crystalline spherical precipitates of 15–20 nm in size. Their crystalline structure may be metastable as they are not consistent with any Y-Ti-O or Ti-O structure. Such detailed observations in the as-milled grain powder confirm a mechanism of Y, Ti, O dissolution in the ferritic matrix followed by a NC precipitation during the mechanical alloying process of ODS materials.
•We observed an ODS ball-milled powder by high resolution transmission microscopy.•The ODS ball-milled powder exhibits a lamellar microstructure.•Small crystalline nanoclusters were detected in the milled ODS powder.•The nanoclusters in the ODS milled powder are enriched in titanium.•Larger NCs of 15–20 nm in size are, at least, partly coherent with the matrix.</description><subject>Ball-milling</subject><subject>Engineering Sciences</subject><subject>Materials</subject><subject>Nanostructured materials</subject><subject>ODS ferritic steel</subject><subject>Powder characterization</subject><subject>Transmission Electron Microscopy</subject><issn>0022-3115</issn><issn>1873-4820</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2016</creationdate><recordtype>article</recordtype><recordid>eNqFUF1LwzAUDaLgnP4Eoa8-tN60TT-eZIzphIkv8zlkye2a0jUj6ebmrzfdhq_Chft1zoFzCHmkEFGg2XMTNd1ObkQfxX6NwBeDKzKiRZ6EaRHDNRkBxHGYUMpuyZ1zDQCwEtiIHOZ6XQcWnWl3vTZdsLSicxvt3LDMWpS99cOHltY4abbHQNbCCtmj1T_ixDBVIIKNbltUgTlohYHSbov2pOB6i926r7HzX9cjtsHWfCu09-SmEq3Dh0sfk6_X2XI6Dxefb-_TySKUKZR9mGb5CiTkRaWYKleqZGlZ0HJFc8WyRGSFFCVlWcqqCqUQqYpFEg_eEsiToiySMXk669ai5VurN8IeuRGazycLPtyAph6cJnvqseyMHcw6i9UfgQIfouYNv0TNh6g5-GLgeS9nHnoje42WO6mxk6i09QFyZfQ_Cr__IIyb</recordid><startdate>20161001</startdate><enddate>20161001</enddate><creator>Loyer-Prost, M.</creator><creator>Merot, J.-S.</creator><creator>Ribis, J.</creator><creator>Le Bouar, Y.</creator><creator>Chaffron, L.</creator><creator>Legendre, F.</creator><general>Elsevier B.V</general><general>Elsevier</general><scope>AAYXX</scope><scope>CITATION</scope><scope>1XC</scope></search><sort><creationdate>20161001</creationdate><title>High resolution Transmission Electron Microscopy characterization of a milled oxide dispersion strengthened steel powder</title><author>Loyer-Prost, M. ; Merot, J.-S. ; Ribis, J. ; Le Bouar, Y. ; Chaffron, L. ; Legendre, F.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c409t-467b0c078fd5d9bd9549819b17d563a68ca915645ffecaa4d2a32059030738983</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2016</creationdate><topic>Ball-milling</topic><topic>Engineering Sciences</topic><topic>Materials</topic><topic>Nanostructured materials</topic><topic>ODS ferritic steel</topic><topic>Powder characterization</topic><topic>Transmission Electron Microscopy</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Loyer-Prost, M.</creatorcontrib><creatorcontrib>Merot, J.-S.</creatorcontrib><creatorcontrib>Ribis, J.</creatorcontrib><creatorcontrib>Le Bouar, Y.</creatorcontrib><creatorcontrib>Chaffron, L.</creatorcontrib><creatorcontrib>Legendre, F.</creatorcontrib><collection>CrossRef</collection><collection>Hyper Article en Ligne (HAL)</collection><jtitle>Journal of nuclear materials</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Loyer-Prost, M.</au><au>Merot, J.-S.</au><au>Ribis, J.</au><au>Le Bouar, Y.</au><au>Chaffron, L.</au><au>Legendre, F.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>High resolution Transmission Electron Microscopy characterization of a milled oxide dispersion strengthened steel powder</atitle><jtitle>Journal of nuclear materials</jtitle><date>2016-10-01</date><risdate>2016</risdate><volume>479</volume><spage>76</spage><epage>84</epage><pages>76-84</pages><issn>0022-3115</issn><eissn>1873-4820</eissn><abstract>Oxide Dispersion Strengthened (ODS) steels are promising materials for generation IV fuel claddings as their dense nano-oxide dispersion provides good creep and irradiation resistance. Even if they have been studied for years, the formation mechanism of these nano-oxides is still unclear. Here we report for the first time a High Resolution Transmission Electron Microscopy and Energy Filtered Transmission Electron Microscopy characterization of an ODS milled powder. It provides clear evidence of the presence of small crystalline nanoclusters (NCs) enriched in titanium directly after milling. Small NCs (<5 nm) have a crystalline structure and seem partly coherent with the matrix. They have an interplanar spacing close to the (011) bcc iron structure. They coexist with larger crystalline spherical precipitates of 15–20 nm in size. Their crystalline structure may be metastable as they are not consistent with any Y-Ti-O or Ti-O structure. Such detailed observations in the as-milled grain powder confirm a mechanism of Y, Ti, O dissolution in the ferritic matrix followed by a NC precipitation during the mechanical alloying process of ODS materials.
•We observed an ODS ball-milled powder by high resolution transmission microscopy.•The ODS ball-milled powder exhibits a lamellar microstructure.•Small crystalline nanoclusters were detected in the milled ODS powder.•The nanoclusters in the ODS milled powder are enriched in titanium.•Larger NCs of 15–20 nm in size are, at least, partly coherent with the matrix.</abstract><pub>Elsevier B.V</pub><doi>10.1016/j.jnucmat.2016.06.050</doi><tpages>9</tpages></addata></record> |
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subjects | Ball-milling Engineering Sciences Materials Nanostructured materials ODS ferritic steel Powder characterization Transmission Electron Microscopy |
title | High resolution Transmission Electron Microscopy characterization of a milled oxide dispersion strengthened steel powder |
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