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Surface graphitization of ozone-treated detonation nanodiamonds
Bifunctional detonation nanodiamonds (NDs) were obtained by vacuum annealing at 750 °C of NDs previously oxidized in ozone (ND‐ozone). Raman investigations demonstrate a significantly higher amount of sp2 carbon compared to ND with polyfunctional surface (ND‐NRI) annealed in vacuum under the same co...
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Published in: | Physica status solidi. A, Applications and materials science Applications and materials science, 2014-12, Vol.211 (12), p.2739-2743 |
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creator | Arnault, Jean-Charles Petit, Tristan Girard, Hugues A. Gesset, Celine Combis-Schlumberger, Mathilde Sennour, Mohammed Koscheev, Alex Khomich, Andrei A. Vlasov, Igor Shenderova, Olga |
description | Bifunctional detonation nanodiamonds (NDs) were obtained by vacuum annealing at 750 °C of NDs previously oxidized in ozone (ND‐ozone). Raman investigations demonstrate a significantly higher amount of sp2 carbon compared to ND with polyfunctional surface (ND‐NRI) annealed in vacuum under the same conditions. In addition to sp2 carbon caps, thermal desorption mass spectroscopy analysis revealed a higher oxygen concentration at the ND‐ozone surface with abundant carbonyl and carboxylic acid anhydride groups. The supernatant of ND‐ozone annealed in vacuum exhibits a positive zeta potential (+50 mV at pH 6.5), while the starting sample has a high negative zeta potential (−60 mV). This supports the oxygen hole‐doping model previously proposed to explain the positive zeta potential of NDs after vacuum annealing. |
doi_str_mv | 10.1002/pssa.201431397 |
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Raman investigations demonstrate a significantly higher amount of sp2 carbon compared to ND with polyfunctional surface (ND‐NRI) annealed in vacuum under the same conditions. In addition to sp2 carbon caps, thermal desorption mass spectroscopy analysis revealed a higher oxygen concentration at the ND‐ozone surface with abundant carbonyl and carboxylic acid anhydride groups. The supernatant of ND‐ozone annealed in vacuum exhibits a positive zeta potential (+50 mV at pH 6.5), while the starting sample has a high negative zeta potential (−60 mV). 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A, Applications and materials science</title><addtitle>Phys. Status Solidi A</addtitle><description>Bifunctional detonation nanodiamonds (NDs) were obtained by vacuum annealing at 750 °C of NDs previously oxidized in ozone (ND‐ozone). Raman investigations demonstrate a significantly higher amount of sp2 carbon compared to ND with polyfunctional surface (ND‐NRI) annealed in vacuum under the same conditions. In addition to sp2 carbon caps, thermal desorption mass spectroscopy analysis revealed a higher oxygen concentration at the ND‐ozone surface with abundant carbonyl and carboxylic acid anhydride groups. The supernatant of ND‐ozone annealed in vacuum exhibits a positive zeta potential (+50 mV at pH 6.5), while the starting sample has a high negative zeta potential (−60 mV). This supports the oxygen hole‐doping model previously proposed to explain the positive zeta potential of NDs after vacuum annealing.</description><subject>Annealing</subject><subject>Carbon</subject><subject>Detonation</subject><subject>diamond</subject><subject>Engineering Sciences</subject><subject>graphitization</subject><subject>Mass spectroscopy</subject><subject>Materials</subject><subject>Micro and nanotechnologies</subject><subject>Microelectronics</subject><subject>nanocrystals</subject><subject>Nanostructure</subject><subject>Neodymium</subject><subject>ozone</subject><subject>reconstruction</subject><subject>surfaces</subject><subject>Vacuum annealing</subject><subject>Zeta potential</subject><issn>1862-6300</issn><issn>0031-8965</issn><issn>1862-6319</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2014</creationdate><recordtype>article</recordtype><recordid>eNqFkElPwzAQRiMEEuuVcyUucEjxeI1PqKJQkApUKsvRcpMJGNK42Cnbr6dVUIW4cBpr_J5n_CXJPpAuEEKPZzHaLiXAGTCt1pItyCRNJQO9vjoTsplsx_hMCBdcwVZyMp6H0ubYeQx29uQa92Ub5-uOLzv-y9eYNgFtg0WnwMbX7V1ta184O_V1EXeTjdJWEfd-6k5yd352e3qRDm8Gl6e9YZozTVVqYWIlSlSiEBM9UVZmyLgmXHOpQFDGCk5yKjgwknEQnNOMc4EqUyWSXLCd5Kh998lWZhbc1IZP460zF72hWfYIAKFcqTdYsIctOwv-dY6xMVMXc6wqW6OfRwMqk6AY42qBHvxBn_081IufGJCMMy0pXQ7vtlQefIwBy9UGQMwye7PM3qyyXwi6Fd5dhZ__0GY0Hvd-u2nrutjgx8q14cVIxZQwD9cD07_vn48errTps28WOZT0</recordid><startdate>201412</startdate><enddate>201412</enddate><creator>Arnault, Jean-Charles</creator><creator>Petit, Tristan</creator><creator>Girard, Hugues A.</creator><creator>Gesset, Celine</creator><creator>Combis-Schlumberger, Mathilde</creator><creator>Sennour, Mohammed</creator><creator>Koscheev, Alex</creator><creator>Khomich, Andrei A.</creator><creator>Vlasov, Igor</creator><creator>Shenderova, Olga</creator><general>Blackwell Publishing Ltd</general><general>Wiley Subscription Services, Inc</general><general>Wiley</general><scope>BSCLL</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SP</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><scope>L7M</scope><scope>1XC</scope><scope>VOOES</scope><orcidid>https://orcid.org/0000-0002-1081-3449</orcidid><orcidid>https://orcid.org/0000-0002-2885-5866</orcidid><orcidid>https://orcid.org/0000-0001-8491-0412</orcidid></search><sort><creationdate>201412</creationdate><title>Surface graphitization of ozone-treated detonation nanodiamonds</title><author>Arnault, Jean-Charles ; Petit, Tristan ; Girard, Hugues A. ; Gesset, Celine ; Combis-Schlumberger, Mathilde ; Sennour, Mohammed ; Koscheev, Alex ; Khomich, Andrei A. ; Vlasov, Igor ; Shenderova, Olga</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c3927-a1ba6e6e75d5b9b7a68e34904946715233d40c25413084154428445e787fe0c53</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2014</creationdate><topic>Annealing</topic><topic>Carbon</topic><topic>Detonation</topic><topic>diamond</topic><topic>Engineering Sciences</topic><topic>graphitization</topic><topic>Mass spectroscopy</topic><topic>Materials</topic><topic>Micro and nanotechnologies</topic><topic>Microelectronics</topic><topic>nanocrystals</topic><topic>Nanostructure</topic><topic>Neodymium</topic><topic>ozone</topic><topic>reconstruction</topic><topic>surfaces</topic><topic>Vacuum annealing</topic><topic>Zeta potential</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Arnault, Jean-Charles</creatorcontrib><creatorcontrib>Petit, Tristan</creatorcontrib><creatorcontrib>Girard, Hugues A.</creatorcontrib><creatorcontrib>Gesset, Celine</creatorcontrib><creatorcontrib>Combis-Schlumberger, Mathilde</creatorcontrib><creatorcontrib>Sennour, Mohammed</creatorcontrib><creatorcontrib>Koscheev, Alex</creatorcontrib><creatorcontrib>Khomich, Andrei A.</creatorcontrib><creatorcontrib>Vlasov, Igor</creatorcontrib><creatorcontrib>Shenderova, Olga</creatorcontrib><collection>Istex</collection><collection>CrossRef</collection><collection>Electronics & Communications Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>Hyper Article en Ligne (HAL)</collection><collection>Hyper Article en Ligne (HAL) (Open Access)</collection><jtitle>Physica status solidi. A, Applications and materials science</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Arnault, Jean-Charles</au><au>Petit, Tristan</au><au>Girard, Hugues A.</au><au>Gesset, Celine</au><au>Combis-Schlumberger, Mathilde</au><au>Sennour, Mohammed</au><au>Koscheev, Alex</au><au>Khomich, Andrei A.</au><au>Vlasov, Igor</au><au>Shenderova, Olga</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Surface graphitization of ozone-treated detonation nanodiamonds</atitle><jtitle>Physica status solidi. A, Applications and materials science</jtitle><addtitle>Phys. Status Solidi A</addtitle><date>2014-12</date><risdate>2014</risdate><volume>211</volume><issue>12</issue><spage>2739</spage><epage>2743</epage><pages>2739-2743</pages><issn>1862-6300</issn><issn>0031-8965</issn><eissn>1862-6319</eissn><notes>ArticleID:PSSA201431397</notes><notes>Russian Academy of Sciences</notes><notes>ark:/67375/WNG-DVDFPWM9-D</notes><notes>Russian Foundation of Basic Research - No. 13-03-01287</notes><notes>istex:B916E09C1EE21423E5624AF8FB89D4DC87437E12</notes><notes>ObjectType-Article-1</notes><notes>SourceType-Scholarly Journals-1</notes><notes>ObjectType-Feature-2</notes><notes>content type line 23</notes><abstract>Bifunctional detonation nanodiamonds (NDs) were obtained by vacuum annealing at 750 °C of NDs previously oxidized in ozone (ND‐ozone). Raman investigations demonstrate a significantly higher amount of sp2 carbon compared to ND with polyfunctional surface (ND‐NRI) annealed in vacuum under the same conditions. In addition to sp2 carbon caps, thermal desorption mass spectroscopy analysis revealed a higher oxygen concentration at the ND‐ozone surface with abundant carbonyl and carboxylic acid anhydride groups. The supernatant of ND‐ozone annealed in vacuum exhibits a positive zeta potential (+50 mV at pH 6.5), while the starting sample has a high negative zeta potential (−60 mV). This supports the oxygen hole‐doping model previously proposed to explain the positive zeta potential of NDs after vacuum annealing.</abstract><cop>Weinheim</cop><pub>Blackwell Publishing Ltd</pub><doi>10.1002/pssa.201431397</doi><tpages>5</tpages><orcidid>https://orcid.org/0000-0002-1081-3449</orcidid><orcidid>https://orcid.org/0000-0002-2885-5866</orcidid><orcidid>https://orcid.org/0000-0001-8491-0412</orcidid><oa>free_for_read</oa></addata></record> |
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subjects | Annealing Carbon Detonation diamond Engineering Sciences graphitization Mass spectroscopy Materials Micro and nanotechnologies Microelectronics nanocrystals Nanostructure Neodymium ozone reconstruction surfaces Vacuum annealing Zeta potential |
title | Surface graphitization of ozone-treated detonation nanodiamonds |
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